2,2'-(4-(hydroxy)-1,3-phenylene)bis(1-(4-chlorophenyl)diazene)

Base Information

• Chemical Name: 2,2'-(4-(hydroxy)-1,3-phenylene)bis(1-(4-chlorophenyl)diazene)
• CAS No.: 1042658-30-9
• Molecular Formula: C₁₈H₁₂Cl₂N₄O
• Molecular Weight: 371.225
• Mol file: 1042658-30-9.mol

Synonyms:2,2'-(4-(hydroxy)-1,3-phenylene)bis(1-(4-chlorophenyl)diazene)

Chemical Property of 2,2'-(4-(hydroxy)-1,3-phenylene)bis(1-(4-chlorophenyl)diazene)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2'-(4-(hydroxy)-1,3-phenylene)bis(1-(4-chlorophenyl)diazene)

There total 6 articles about 2,2'-(4-(hydroxy)-1,3-phenylene)bis(1-(4-chlorophenyl)diazene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

4-chloro-aniline (106-47-8) + phenol (108-95-2,27073-41-2) → 2,2'-(4-(hydroxy)-1,3-phenylene)bis(1-(4-chlorophenyl)diazene) (1042658-30-9)

Guidance literature:

4-chloro-aniline; With hydrogenchloride; sodium nitrite; In water; at 0 - 5 ℃;

phenol; With sodium hydroxide; In water;

DOI:10.1016/j.molstruc.2007.08.037

Reference yield:

p-chlorobenzenediazonium chloride (2028-74-2) → 2,2'-(4-(hydroxy)-1,3-phenylene)bis(1-(4-chlorophenyl)diazene) (1042658-30-9)

Guidance literature:

Multi-step reaction with 2 steps

1: alkali

2: alkali

With alkali;

Reference yield:

phenol (108-95-2,27073-41-2) → 2,2'-(4-(hydroxy)-1,3-phenylene)bis(1-(4-chlorophenyl)diazene) (1042658-30-9)

Guidance literature:

Multi-step reaction with 2 steps

1: alkali

2: alkali

With alkali;

upstream raw materials:

2-(4-chloro-phenylazo)-phenol

p-chlorobenzenediazonium chloride

4-chloro-4'-hydroxyazobenzene

phenol

Downstream raw materials:

2,2'-(4-(octyloxy)-1,3-phenylene)bis(1-(4-chlorophenyl)diazene)

C₂₈H₃₂Cl₂N₄O

C₃₂H₄₀Cl₂N₄O

C₃₀H₃₆Cl₂N₄O