N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] nonanamide

Base Information

Chemical Name:N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] nonanamide
CAS No.:1449203-92-2
Molecular Formula:C₁₈H₂₄IN₃O₃S
Molecular Weight:489.377
Hs Code.:

Synonyms:N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] nonanamide

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Chemical Property of N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] nonanamide

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Technology Process of N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] nonanamide

There total 7 articles about N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] nonanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.85%

: C₂₇H₄₀IN₃O₄S

: 1449203-92-2
N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] nonanamide

Guidance literature:: With methanol; sodium hydroxide; for 3h; Reflux;

Reference yield:

: 5438-36-8
5-iodovaniline

: 1449203-92-2
N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] nonanamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid / 4 h / 20 °C

2.1: acetic acid / methanol / 6 h / pH 4 - 5 / Reflux

3.1: iron(III) chloride / methanol; water / Reflux

3.2: 1 h / Reflux

4.1: pyridine / 2 h / 20 °C

5.1: sodium hydroxide / methanol / 3 h / Reflux

With pyridine; iron(III) chloride; sulfuric acid; acetic acid; sodium hydroxide; In methanol; water;
DOI:10.1016/j.ejmech.2013.05.001

Reference yield:

: 486994-14-3
4-(acetyloxy)-3-iodo-5-methoxybenzaldehyde

: 1449203-92-2
N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] nonanamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / methanol / 6 h / pH 4 - 5 / Reflux

2.1: iron(III) chloride / methanol; water / Reflux

2.2: 1 h / Reflux

3.1: pyridine / 2 h / 20 °C

4.1: sodium hydroxide / methanol / 3 h / Reflux

With pyridine; iron(III) chloride; acetic acid; sodium hydroxide; In methanol; water;
DOI:10.1016/j.ejmech.2013.05.001