m-(benzyloxycarbonyl)phenyl acetic acid

Base Information

Chemical Name:m-(benzyloxycarbonyl)phenyl acetic acid
CAS No.:113266-90-3
Molecular Formula:C₁₆H₁₄O₄
Molecular Weight:270.285
Hs Code.:

Synonyms:m-(benzyloxycarbonyl)phenyl acetic acid

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Chemical Property of m-(benzyloxycarbonyl)phenyl acetic acid

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Technology Process of m-(benzyloxycarbonyl)phenyl acetic acid

There total 7 articles about m-(benzyloxycarbonyl)phenyl acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 113266-89-0
2,2,2-trichloroethyl-phenyl acetate

: 113266-90-3
m-(benzyloxycarbonyl)phenyl acetic acid

Guidance literature:: With acetic acid; zinc; In tetrahydrofuran; at 0 ℃; for 3h;
DOI:10.1021/jm000145g

Reference yield: 37.0%

: aqueous potassium dihydrogen phosphate (KH₂PO₄)

: 59819-52-2
2,2,2-trichloroethyl 2-chlorophenyl phosphorochloridate

: 113266-90-3
m-(benzyloxycarbonyl)phenyl acetic acid

Guidance literature:: With hydrogenchloride; zinc; In tetrahydrofuran; chloroform;

Reference yield:

: 121-91-5
isophthalic acid

: 113266-90-3
m-(benzyloxycarbonyl)phenyl acetic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: Et₃N / methanol; H₂O

1.2: 49 percent / dimethylformamide / 2 h / 100 °C

2.1: oxalyl chloride / DMF / CH₂Cl₂ / 1 h / 20 °C

3.1: diethyl ether; benzene / 0.5 h / cooling

4.1: 68 percent / Ag₂O / 0.5 h / 50 - 60 °C

5.1: 84 percent / aq. AcOH; Zn / tetrahydrofuran / 3 h / 0 °C

With oxalyl dichloride; acetic acid; triethylamine; silver(l) oxide; zinc; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; benzene; 4.1: Arndt-Eistert homologation;
DOI:10.1021/jm000145g