phosphoric acid di-tert-butyl ester 4-{2-[4-((E)-6-iodohex-5-enyloxy)phenyl]ethyl}-2-methyl-4,5-dihydrooxazol-4-yl methyl ester

Base Information

Chemical Name:phosphoric acid di-tert-butyl ester 4-{2-[4-((E)-6-iodohex-5-enyloxy)phenyl]ethyl}-2-methyl-4,5-dihydrooxazol-4-yl methyl ester
CAS No.:1301696-77-4
Molecular Formula:C₂₇H₄₃INO₆P
Molecular Weight:635.52
Hs Code.:

Synonyms:phosphoric acid di-tert-butyl ester 4-{2-[4-((E)-6-iodohex-5-enyloxy)phenyl]ethyl}-2-methyl-4,5-dihydrooxazol-4-yl methyl ester

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Chemical Property of phosphoric acid di-tert-butyl ester 4-{2-[4-((E)-6-iodohex-5-enyloxy)phenyl]ethyl}-2-methyl-4,5-dihydrooxazol-4-yl methyl ester

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Technology Process of phosphoric acid di-tert-butyl ester 4-{2-[4-((E)-6-iodohex-5-enyloxy)phenyl]ethyl}-2-methyl-4,5-dihydrooxazol-4-yl methyl ester

There total 7 articles about phosphoric acid di-tert-butyl ester 4-{2-[4-((E)-6-iodohex-5-enyloxy)phenyl]ethyl}-2-methyl-4,5-dihydrooxazol-4-yl methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1301696-62-7
(4-{2-[4-((E)-6-iodohex-5-enyloxy)phenyl]ethyl}-2-methyl-4,5-dihydrooxazol-4-yl)methanol

: 117924-33-1
di-tert-butyl N,N-diethylphosphoramidite

: 1301696-77-4
phosphoric acid di-tert-butyl ester 4-{2-[4-((E)-6-iodohex-5-enyloxy)phenyl]ethyl}-2-methyl-4,5-dihydrooxazol-4-yl methyl ester

Guidance literature:: (4-{2-[4-((E)-6-iodohex-5-enyloxy)phenyl]ethyl}-2-methyl-4,5-dihydrooxazol-4-yl)methanol; di-tert-butyl N,N-diethylphosphoramidite; With 1H-tetrazole; In tetrahydrofuran; dichloromethane; at 20 ℃; for 6h;

With dihydrogen peroxide; In tetrahydrofuran; dichloromethane; water; at 20 ℃; for 1.5h;

Reference yield:

: C₂₇H₄₃INO₅P

: 1301696-77-4
phosphoric acid di-tert-butyl ester 4-{2-[4-((E)-6-iodohex-5-enyloxy)phenyl]ethyl}-2-methyl-4,5-dihydrooxazol-4-yl methyl ester

Guidance literature:: With dihydrogen peroxide; In tetrahydrofuran; dichloromethane; water; at 20 ℃; for 1.5h;
DOI:10.1002/cmdc.201000477

Reference yield:

: 201035-80-5
(E)-6-iodohex-5-en-1-ol

: 1301696-77-4
phosphoric acid di-tert-butyl ester 4-{2-[4-((E)-6-iodohex-5-enyloxy)phenyl]ethyl}-2-methyl-4,5-dihydrooxazol-4-yl methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 115 h / 20 - 50 °C

2.1: 1H-tetrazole / dichloromethane; tetrahydrofuran / 6 h / 20 °C

2.2: 1.5 h / 20 °C

With 1H-tetrazole; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; dichloromethane;