C₄₈H₅₈N₄O₉Si

Base Information

Chemical Name:C₄₈H₅₈N₄O₉Si
CAS No.:1268464-15-8
Molecular Formula:C₄₈H₅₈N₄O₉Si
Molecular Weight:863.095
Hs Code.:

C<sub>48</sub>H<sub>58</sub>N<sub>4</sub>O<sub>9</sub>Si

Synonyms:C₄₈H₅₈N₄O₉Si

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Chemical Property of C₄₈H₅₈N₄O₉Si

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Technology Process of C₄₈H₅₈N₄O₉Si

There total 13 articles about C₄₈H₅₈N₄O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1268463-62-2
C₄₇H₅₆N₄O₉Si

: 1268464-15-8
C₄₈H₅₈N₄O₉Si

Guidance literature:: formaldehyd; C₄₇H₅₆N₄O₉Si; With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; at 23 ℃; for 0.583333h;

With sodium hydrogencarbonate; In water; 1,2-dichloro-ethane; pH=7; Phosphate buffer;

Reference yield:

: 2785-98-0
2,5-dimethoxybenzoic acid

: 1268464-15-8
C₄₈H₅₈N₄O₉Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: 2,2,6,6-tetramethyl-piperidine; n-butyllithium / tetrahydrofuran / 2.5 h / 0 °C

1.2: 2 h / 25 °C

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 25 °C

3.1: dmap; triethylamine / dichloromethane / 12 h / 25 °C

4.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C

5.2: 20 °C

6.1: acetic anhydride; copper(II) nitrate hydrate / 3 h / 0 - 20 °C

7.1: sodium dithionite / water; tetrahydrofuran / 20 °C

8.1: dmap / N,N-dimethyl-formamide / 5 h / 20 °C

9.1: N,N,N,N,-tetramethylethylenediamine; diisopropylamine; n-butyllithium / tetrahydrofuran; hexanes / 0.5 h / -78 °C

9.2: 2 h / -100 - -20 °C

10.1: hydrogenchloride / 1,4-dioxane / 20 °C

11.1: dichloromethane; tetrahydrofuran / 20 °C

12.1: potassium carbonate / water; tetrahydrofuran; methanol / 20 °C

13.1: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 0.58 h / 23 °C

13.2: pH 7 / Phosphate buffer

With 2,2,6,6-tetramethyl-piperidine; hydrogenchloride; dmap; n-butyllithium; sodium dithionite; oxalyl dichloride; copper(II) nitrate hydrate; N,N,N,N,-tetramethylethylenediamine; acetic anhydride; boron tribromide; sodium tris(acetoxy)borohydride; sodium hydride; potassium carbonate; acetic acid; triethylamine; diisopropylamine; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; methanol; hexanes; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 116324-66-4
2,5-Dimethoxy-6-methylbenzoesaeure

: 1268464-15-8
C₄₈H₅₈N₄O₉Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 25 °C

2.1: dmap; triethylamine / dichloromethane / 12 h / 25 °C

3.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C

4.2: 20 °C

5.1: acetic anhydride; copper(II) nitrate hydrate / 3 h / 0 - 20 °C

6.1: sodium dithionite / water; tetrahydrofuran / 20 °C

7.1: dmap / N,N-dimethyl-formamide / 5 h / 20 °C

8.1: N,N,N,N,-tetramethylethylenediamine; diisopropylamine; n-butyllithium / tetrahydrofuran; hexanes / 0.5 h / -78 °C

8.2: 2 h / -100 - -20 °C

9.1: hydrogenchloride / 1,4-dioxane / 20 °C

10.1: dichloromethane; tetrahydrofuran / 20 °C

11.1: potassium carbonate / water; tetrahydrofuran; methanol / 20 °C

12.1: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 0.58 h / 23 °C

12.2: pH 7 / Phosphate buffer

With hydrogenchloride; dmap; n-butyllithium; sodium dithionite; oxalyl dichloride; copper(II) nitrate hydrate; N,N,N,N,-tetramethylethylenediamine; acetic anhydride; boron tribromide; sodium tris(acetoxy)borohydride; sodium hydride; potassium carbonate; acetic acid; triethylamine; diisopropylamine; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; methanol; hexanes; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;