2,2-Difluoro-4,6-dimethyl-2H-1,3,2-dioxaborinin-1-ium-2-uide

Base Information

Chemical Name:2,2-Difluoro-4,6-dimethyl-2H-1,3,2-dioxaborinin-1-ium-2-uide
CAS No.:15390-25-7
Molecular Formula:C5H7 B F2 O2
Molecular Weight:147.917
Hs Code.:
Nikkaji Number:J2.174.475A

Synonyms:2,2-DIFLUORO-4,6-DIMETHYL-2H-1,3,2-DIOXABORININ-1-IUM-2-UIDE;15390-25-7;MFCD07756755;AKOS002263160;E87337

Suppliers and Price of 2,2-Difluoro-4,6-dimethyl-2H-1,3,2-dioxaborinin-1-ium-2-uide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2,2-Difluoro-4,6-dimethyl-2H-1,3,2-dioxaborinin-1-ium-2-uide

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:148.0507160
Heavy Atom Count:10
Complexity:191

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:[B-]1(OC(=CC(=[O+]1)C)C)(F)F

Technology Process of 2,2-Difluoro-4,6-dimethyl-2H-1,3,2-dioxaborinin-1-ium-2-uide

There total 1 articles about 2,2-Difluoro-4,6-dimethyl-2H-1,3,2-dioxaborinin-1-ium-2-uide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 2,4-pentanedionato-κC3(2,4-pentanedionato-κ2-O,O')triphenylphosphanepalladium(II)

: 109-63-7
boron trifluoride diethyl etherate

: 603-35-0
triphenylphosphine

: 33680-09-0
(2,4-pentanedionato-κ2-O,O')bis(triphenylphosphane)palladium(II) tetrafluoroborate

: 15390-25-7
(acetylacetonato)borondifluoride

Guidance literature:: In benzene; under Ar; PPh3 and Pd(acac)2(PPh3) dissolved in benzene at room temp.; BF3(OEt2) added dropwise via syringe under vigorous stirring; ppt. filtered off under Ar, washed with benzene, dried at room temp. under vac.; elem. anal.;
DOI:10.1134/S1070328411090119