(2,4-pentanedionato-κ2-O,O')bis(triphenylphosphane)palladium(II) tetrafluoroborate

Base Information

Chemical Name:(2,4-pentanedionato-κ2-O,O')bis(triphenylphosphane)palladium(II) tetrafluoroborate
CAS No.:33680-09-0
Molecular Formula:BF₄*C₄₁H₃₇O₂P₂Pd
Molecular Weight:816.916
Hs Code.:

Synonyms:(2,4-pentanedionato-κ2-O,O')bis(triphenylphosphane)palladium(II) tetrafluoroborate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2,4-pentanedionato-κ2-O,O')bis(triphenylphosphane)palladium(II) tetrafluoroborate

Chemical Property:

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Technology Process of (2,4-pentanedionato-κ2-O,O')bis(triphenylphosphane)palladium(II) tetrafluoroborate

There total 10 articles about (2,4-pentanedionato-κ2-O,O')bis(triphenylphosphane)palladium(II) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 80583-63-7
tetrakis(triphenylphosphine)palladium(II) tetrafluoroborate-acetone (1/1)

: 1118-67-8
sodium (Z)-4-oxopent-2-en-2-olate

: 33680-09-0
bis(triphenylphosphine)(acetylacetonato)palladium(II) tetrafluoroborate-acetone (1/1)

Guidance literature:: In ethanol; acetone; reaction of equimolar amounts in warmed CH3OH-acetone; elem. anal.;
DOI:10.1021/ic00134a072

Reference yield: 96.0%

: 2,4-pentanedionato-κC3(2,4-pentanedionato-κ2-O,O')triphenylphosphanepalladium(II)

: 109-63-7
boron trifluoride diethyl etherate

: 603-35-0
triphenylphosphine

: 33680-09-0
(2,4-pentanedionato-κ2-O,O')bis(triphenylphosphane)palladium(II) tetrafluoroborate

: 15390-25-7
(acetylacetonato)borondifluoride

Guidance literature:: In benzene; under Ar; PPh3 and Pd(acac)2(PPh3) dissolved in benzene at room temp.; BF3(OEt2) added dropwise via syringe under vigorous stirring; ppt. filtered off under Ar, washed with benzene, dried at room temp. under vac.; elem. anal.;
DOI:10.1134/S1070328411090119