4-{4-[4-(3-carboxybenzamido)-1-methyl-1H-pyrrole-2-carboxamido]-1-methyl-1H-pyrrole-2-carboxamido}-1-methyl-1H-pyrrole-2-carboxylic acid

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Chemical Name:4-{4-[4-(3-carboxybenzamido)-1-methyl-1H-pyrrole-2-carboxamido]-1-methyl-1H-pyrrole-2-carboxamido}-1-methyl-1H-pyrrole-2-carboxylic acid
CAS No.:1312790-32-1
Molecular Formula:C₂₆H₂₄N₆O₇
Molecular Weight:532.513
Hs Code.:

Synonyms:4-{4-[4-(3-carboxybenzamido)-1-methyl-1H-pyrrole-2-carboxamido]-1-methyl-1H-pyrrole-2-carboxamido}-1-methyl-1H-pyrrole-2-carboxylic acid

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Chemical Property of 4-{4-[4-(3-carboxybenzamido)-1-methyl-1H-pyrrole-2-carboxamido]-1-methyl-1H-pyrrole-2-carboxamido}-1-methyl-1H-pyrrole-2-carboxylic acid

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Technology Process of 4-{4-[4-(3-carboxybenzamido)-1-methyl-1H-pyrrole-2-carboxamido]-1-methyl-1H-pyrrole-2-carboxamido}-1-methyl-1H-pyrrole-2-carboxylic acid

There total 7 articles about 4-{4-[4-(3-carboxybenzamido)-1-methyl-1H-pyrrole-2-carboxamido]-1-methyl-1H-pyrrole-2-carboxamido}-1-methyl-1H-pyrrole-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1312790-30-9
methyl 4-(4-{4-[3-(methoxycarbonyl)benzamido]-1-methyl-1H-pyrrole-2-carboxamido}-1-methyl-1H-pyrrole-2-carboxamido)-1-methyl-1H-pyrrole-2-carboxylate

: 1312790-32-1
4-{4-[4-(3-carboxybenzamido)-1-methyl-1H-pyrrole-2-carboxamido]-1-methyl-1H-pyrrole-2-carboxamido}-1-methyl-1H-pyrrole-2-carboxylic acid

Guidance literature:: With water; sodium hydroxide; In methanol; at 60 ℃; for 48h;
DOI:10.1055/s-0030-1259980

Reference yield:

: 77716-11-1
4-[(tert-butoxycarbonyl)amino]-1-methyl-1H-pyrrole-2-carboxylic acid

: 1312790-32-1
4-{4-[4-(3-carboxybenzamido)-1-methyl-1H-pyrrole-2-carboxamido]-1-methyl-1H-pyrrole-2-carboxamido}-1-methyl-1H-pyrrole-2-carboxylic acid

Guidance literature:: Multi-step reaction with 6 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 24 h / 20 °C

2: hydrogenchloride; water / ethyl acetate / 24 h / 20 °C

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 24 h / 20 °C

4: hydrogenchloride; water / ethyl acetate / 24 h / 20 °C

5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 24 h / 20 °C

6: water; sodium hydroxide / methanol / 48 h / 60 °C

With hydrogenchloride; dmap; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1055/s-0030-1259980

Reference yield:

: 180258-45-1
methyl 4-amino-1-methyl-pyrrole-2-carboxylate hydrochloride

: 1312790-32-1
4-{4-[4-(3-carboxybenzamido)-1-methyl-1H-pyrrole-2-carboxamido]-1-methyl-1H-pyrrole-2-carboxamido}-1-methyl-1H-pyrrole-2-carboxylic acid

Guidance literature:: Multi-step reaction with 6 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 24 h / 20 °C

2: hydrogenchloride; water / ethyl acetate / 24 h / 20 °C

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 24 h / 20 °C

4: hydrogenchloride; water / ethyl acetate / 24 h / 20 °C

5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 24 h / 20 °C

6: water; sodium hydroxide / methanol / 48 h / 60 °C

With hydrogenchloride; dmap; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1055/s-0030-1259980