[3-(tert-butyl-dimethyl-silanyloxymethyl)-4-chloro-benzyl]-methyl-amine

Base Information

Chemical Name:[3-(tert-butyl-dimethyl-silanyloxymethyl)-4-chloro-benzyl]-methyl-amine
CAS No.:1007392-98-4
Molecular Formula:C₁₅H₂₆ClNOSi
Molecular Weight:299.916
Hs Code.:

Synonyms:[3-(tert-butyl-dimethyl-silanyloxymethyl)-4-chloro-benzyl]-methyl-amine

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Chemical Property of [3-(tert-butyl-dimethyl-silanyloxymethyl)-4-chloro-benzyl]-methyl-amine

Chemical Property:

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Technology Process of [3-(tert-butyl-dimethyl-silanyloxymethyl)-4-chloro-benzyl]-methyl-amine

There total 2 articles about [3-(tert-butyl-dimethyl-silanyloxymethyl)-4-chloro-benzyl]-methyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 946001-15-6
[3-(tert-butyl-dimethyl-silanyloxymethyl)-4-chloro-benzyl]-carbamic acid methyl ester

: 1007392-98-4
[3-(tert-butyl-dimethyl-silanyloxymethyl)-4-chloro-benzyl]-methyl-amine

Guidance literature:: [3-(tert-butyl-dimethyl-silanyloxymethyl)-4-chloro-benzyl]-carbamic acid methyl ester; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃;

With Rochelle's salt; In tetrahydrofuran; water; at 20 ℃; for 2h;

Reference yield:

: 946000-08-4
3-(((tert-butyldimethylsilyl)oxy)methyl)-4-chlorobenzaldehyde

: 74-89-5
methylamine

: 1007392-98-4
[3-(tert-butyl-dimethyl-silanyloxymethyl)-4-chloro-benzyl]-methyl-amine

Guidance literature:: 3-(((tert-butyldimethylsilyl)oxy)methyl)-4-chlorobenzaldehyde; methylamine; In tetrahydrofuran; at 20 ℃; for 16h; Molecular sieve;

With sodium tetrahydroborate; In ethanol; at 20 ℃; for 3h;

With hydrogenchloride; sodium hydroxide; ethanol; water; more than 3 stages;

Reference yield:

: 1007392-98-4
[3-(tert-butyl-dimethyl-silanyloxymethyl)-4-chloro-benzyl]-methyl-amine

: 108-24-7
acetic anhydride

: N-[3-({[tert-butyl(dimethyl)silyl]oxy}methyl)-4-chlorobenzyl]-N-methylacetamide

Guidance literature:: [3-(tert-butyl-dimethyl-silanyloxymethyl)-4-chloro-benzyl]-methyl-amine; acetic anhydride; With pyridine; at 20 ℃; for 3h;

With sodium hydrogencarbonate; In water; ethyl acetate;