Pt(p-tol)₂(cod)

Base Information

Chemical Name:Pt(p-tol)₂(cod)
CAS No.:54866-11-4
Molecular Formula:C₂₂H₂₆Pt
Molecular Weight:485.528
Hs Code.:

Synonyms:Pt(p-tol)₂(cod)

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Chemical Property of Pt(p-tol)₂(cod)

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Technology Process of Pt(p-tol)₂(cod)

There total 2 articles about Pt(p-tol)₂(cod) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 12080-32-9
dichloro( 1,5-cyclooctadiene)platinum(ll)

: 4294-57-9
para-methylphenylmagnesium bromide

: 54866-11-4
Pt(p-tol)₂(cod)

Guidance literature:: With ammonium chloride; In diethyl ether; 4-MeC6H4MgBr was added to soln. (COD)PtCl2 in ether, wad stirred at roomtemp. for 12 h under inert atm.; aq. NH4Cl was added, ether layer was dried over MgSO4, filtered through Celite and carbon, and evapd., residue was recrystd. from CH2Cl2/pentane;
DOI:10.1021/ja0480365

Reference yield: 48.0%

: [(Pt(C6H4Me-4)(cod))2(μ-OH)](BF4)

: 54866-11-4
Pt(p-tol)₂(cod)

Guidance literature:: With tetra(n-butyl)ammonium hydroxide; In tetrahydrofuran; room temp.;
DOI:10.1016/j.jorganchem.2006.05.064

Reference yield: 95.0%

: 12150-46-8
1,1'-bis-(diphenylphosphino)ferrocene

: 54866-11-4
Pt(p-tol)₂(cod)

: 791838-70-5
(1,1'-bis(diphenylphosphino)ferrocene)Pt(C₆H₄-4-Me)2

Guidance literature:: In benzene; DPPF was added to soln.(COD)Pt(C6H4-4-Me)2 in benzene and stirred for 1 h at room temp. under inert atm.; solvent was evapd. under reduced pressure, solid was recrystd. from CH2Cl2-pentane; elem.anal.;
DOI:10.1021/ja0480365