S-phenyl naphthalene-1-carbothioate

Base Information

Chemical Name:S-phenyl naphthalene-1-carbothioate
CAS No.:24197-80-6
Molecular Formula:C₁₇H₁₂OS
Molecular Weight:264.348
Hs Code.:

Synonyms:S-phenyl naphthalene-1-carbothioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S-phenyl naphthalene-1-carbothioate

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Technology Process of S-phenyl naphthalene-1-carbothioate

There total 6 articles about S-phenyl naphthalene-1-carbothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 201230-82-2
carbon monoxide

: 90-14-2
1-Iodonaphthalene

: 108-98-5
thiophenol

: 24197-80-6
S-phenyl naphthalene-1-carbothioate

Guidance literature:: With triethylamine; triphenylphosphine; palladium diacetate; at 100 ℃; for 18h; under 10343.2 Torr;
DOI:10.1021/jo800287s

Reference yield: 85.0%

: 4551-15-9
phenylthiotrimethylsilane

: 879-18-5
naphthalene-1-carbonic acid chloride

: 24197-80-6
S-phenyl naphthalene-1-carbothioate

Guidance literature:: In chloroform; at 50 ℃; for 4h;
DOI:10.1055/s-1981-29522

Reference yield: 63.0%

: 90-11-9
1-Bromonaphthalene

: 108-98-5
thiophenol

: 82102-37-2
9-methyl-9H-fluorene-9-carbonyl chloride

: 24197-80-6
S-phenyl naphthalene-1-carbothioate

Guidance literature:: 1-Bromonaphthalene; thiophenol; With bis(benzonitrile)palladium(II) dichloride; sodium acetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium iodide; Inert atmosphere; Glovebox;

9-methyl-9H-fluorene-9-carbonyl chloride; With N-Methyldicyclohexylamine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tri tert-butylphosphoniumtetrafluoroborate; at 120 ℃; for 18h; Inert atmosphere; Glovebox;
DOI:10.1021/jo5009965