C₂₁H₂₂N₂O₈S

Base Information

Chemical Name:C₂₁H₂₂N₂O₈S
CAS No.:1262297-42-6
Molecular Formula:C₂₁H₂₂N₂O₈S
Molecular Weight:462.48
Hs Code.:

C<sub>21</sub>H<sub>22</sub>N<sub>2</sub>O<sub>8</sub>S

Synonyms:C₂₁H₂₂N₂O₈S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₂₂N₂O₈S

Chemical Property:

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Technology Process of C₂₁H₂₂N₂O₈S

There total 9 articles about C₂₁H₂₂N₂O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₂₀ClNO₇S

: 1262297-42-6
C₂₁H₂₂N₂O₈S

Guidance literature:: With hydroxylamine hydrochloride; sodium hydrogencarbonate; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield:

: 38323-22-7
dimethyl (4-nitrobenzylidene)malonate

: 1262297-42-6
C₂₁H₂₂N₂O₈S

Guidance literature:: Multi-step reaction with 5 steps

1: sodium cyanoborohydride / methanol / 20 °C

2: hydrogen / palladium 10% on activated carbon / methanol / 20 °C

3: pyridine / dichloromethane / 1 h / 40 °C

4: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / Reflux

5: hydroxylamine hydrochloride; sodium hydrogencarbonate / tetrahydrofuran / 1 h / 20 °C

With pyridine; oxalyl dichloride; hydroxylamine hydrochloride; hydrogen; sodium cyanoborohydride; sodium hydrogencarbonate; palladium 10% on activated carbon; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 1262297-42-6
C₂₁H₂₂N₂O₈S

Guidance literature:: Multi-step reaction with 6 steps

1: piperidine; benzoic acid / ethanol / 5 h / Reflux

2: sodium cyanoborohydride / methanol / 20 °C

3: hydrogen / palladium 10% on activated carbon / methanol / 20 °C

4: pyridine / dichloromethane / 1 h / 40 °C

5: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / Reflux

6: hydroxylamine hydrochloride; sodium hydrogencarbonate / tetrahydrofuran / 1 h / 20 °C

With piperidine; pyridine; oxalyl dichloride; hydroxylamine hydrochloride; hydrogen; sodium cyanoborohydride; sodium hydrogencarbonate; benzoic acid; palladium 10% on activated carbon; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; ethanol; dichloromethane;