N'-(4-chlorobenzylidene)-2-nitrobenzenesulfonohydrazide

Base Information

• Chemical Name: N'-(4-chlorobenzylidene)-2-nitrobenzenesulfonohydrazide
• CAS No.: 6655-32-9
• Molecular Formula: C₁₃H₁₀ClN₃O₄S
• Molecular Weight: 339.759
• Mol file: 6655-32-9.mol

Synonyms:N'-(4-chlorobenzylidene)-2-nitrobenzenesulfonohydrazide

Chemical Property of N'-(4-chlorobenzylidene)-2-nitrobenzenesulfonohydrazide

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N'-(4-chlorobenzylidene)-2-nitrobenzenesulfonohydrazide

There total 2 articles about N'-(4-chlorobenzylidene)-2-nitrobenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-nitrobenzenesulfonyl hydrazide (5906-99-0) + 4-chlorobenzaldehyde (104-88-1) → N'-(4-chlorobenzylidene)-2-nitrobenzenesulfonohydrazide (6655-32-9)

Guidance literature:

DOI:10.1039/j39660001229

Reference yield:

2-Nitrobenzenesulfonyl chloride (1694-92-4) → N'-(4-chlorobenzylidene)-2-nitrobenzenesulfonohydrazide (6655-32-9)

Guidance literature:

Multi-step reaction with 2 steps

1: N₂H₄*H₂O

With hydrazine hydrate;

DOI:10.1039/j39660001229

Reference yield: 96.0%

4-nitrosobenzoic acid ethyl ester (7476-79-1) + N'-(4-chlorobenzylidene)-2-nitrobenzenesulfonohydrazide (6655-32-9) → N-(4-ethoxycarbonylphenyl)-α-(4-chlorophenyl)nitrone

Guidance literature:

With sodium hydride; In dichloromethane; mineral oil; at 1340 ℃; for 16h; Inert atmosphere; Sealed tube;

DOI:10.1055/s-0036-1591757

upstream raw materials:

2-nitrobenzenesulfonyl hydrazide

4-chlorobenzaldehyde

2-Nitrobenzenesulfonyl chloride

Downstream raw materials:

(4-chlorobenzyl)triethylsilane

(4-chlorobenzyl)triphenylsilane

4-chlorobenzyltri-n-butylstannane

(E)-1,3-di(4-chlorophenyl)-2-propen-1-one