Technology Process of (4-chlorobenzyl)triphenylsilane
There total 5 articles about (4-chlorobenzyl)triphenylsilane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
N'-(4-chlorobenzylidene)-2-nitrobenzenesulfonohydrazide;
With
sodium hydride;
In
dichloromethane;
at 20 ℃;
for 1h;
Sealed tube;
Glovebox;
Inert atmosphere;
HSiPh3;
With
silver trifluoromethanesulfonate;
In
dichloromethane;
at 80 ℃;
for 24h;
Sealed tube;
Glovebox;
Inert atmosphere;
DOI:10.1039/c6cc09650f
- Guidance literature:
-
With
meso-tetraphenylporphyrin iron(III) chloride; sodium hydride;
In
toluene; mineral oil;
at 80 ℃;
for 14h;
Sealed tube;
Inert atmosphere;
DOI:10.1021/acs.orglett.8b01931
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: methanol / 20 °C
2.1: sodium hydride / dichloromethane / 1 h / 20 °C / Sealed tube; Glovebox; Inert atmosphere
2.2: 24 h / 80 °C / Sealed tube; Glovebox; Inert atmosphere
With
sodium hydride;
In
methanol; dichloromethane;
DOI:10.1039/c6cc09650f
