Stannane, tributyl[(4-chlorophenyl)methyl]-

Base Information

Chemical Name:Stannane, tributyl[(4-chlorophenyl)methyl]-
CAS No.:74260-39-2
Molecular Formula:C19H33ClSn
Molecular Weight:415.634
Hs Code.:
DSSTox Substance ID:DTXSID60464245

Synonyms:Stannane, tributyl[(4-chlorophenyl)methyl]-;74260-39-2;SCHEMBL6781894;DTXSID60464245

Suppliers and Price of Stannane, tributyl[(4-chlorophenyl)methyl]-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Stannane, tributyl[(4-chlorophenyl)methyl]-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:11
Exact Mass:416.129281
Heavy Atom Count:21
Complexity:224

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC[Sn](CCCC)(CCCC)CC1=CC=C(C=C1)Cl

Technology Process of Stannane, tributyl[(4-chlorophenyl)methyl]-

There total 3 articles about Stannane, tributyl[(4-chlorophenyl)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 6655-32-9
N'-(4-chlorobenzylidene)-2-nitrobenzenesulfonohydrazide

: 688-73-3
tri-n-butyl-tin hydride

: 74260-39-2
4-chlorobenzyltri-n-butylstannane

Guidance literature:: N'-(4-chlorobenzylidene)-2-nitrobenzenesulfonohydrazide; With sodium hydride; In dichloromethane; at 20 ℃; for 1h; Sealed tube; Glovebox; Inert atmosphere;

tri-n-butyl-tin hydride; With silver trifluoromethanesulfonate; In dichloromethane; at 80 ℃; for 24h; Sealed tube; Glovebox; Inert atmosphere;
DOI:10.1039/c6cc09650f

Reference yield: 85.0%

: 19350-69-7
4-chlorobenzaldehyde p-toluenesulfonylhydrazone

: 688-73-3
tri-n-butyl-tin hydride

: 74260-39-2
4-chlorobenzyltri-n-butylstannane

Guidance literature:: With meso-tetraphenylporphyrin iron(III) chloride; sodium hydride; In toluene; mineral oil; at 80 ℃; for 14h; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01931

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 74260-39-2
4-chlorobenzyltri-n-butylstannane

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol / 20 °C

2.1: sodium hydride / dichloromethane / 1 h / 20 °C / Sealed tube; Glovebox; Inert atmosphere

2.2: 24 h / 80 °C / Sealed tube; Glovebox; Inert atmosphere

With sodium hydride; In methanol; dichloromethane;
DOI:10.1039/c6cc09650f