5-(2-nitrophenyl)-4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo<8.8.8>hexacosane-2,9-dione

Base Information

Chemical Name:5-(2-nitrophenyl)-4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo<8.8.8>hexacosane-2,9-dione
CAS No.:135949-42-7
Molecular Formula:C₂₄H₃₅N₃O₁₀
Molecular Weight:525.556
Hs Code.:

Synonyms:5-(2-nitrophenyl)-4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo<8.8.8>hexacosane-2,9-dione

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Chemical Property of 5-(2-nitrophenyl)-4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo<8.8.8>hexacosane-2,9-dione

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Technology Process of 5-(2-nitrophenyl)-4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo<8.8.8>hexacosane-2,9-dione

There total 4 articles about 5-(2-nitrophenyl)-4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo<8.8.8>hexacosane-2,9-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 135949-38-1
4-(2-nitrophenyl)-3,6-dioxaoctanedioyl chloride

: 23978-55-4
1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

: 135949-42-7
5-(2-nitrophenyl)-4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo<8.8.8>hexacosane-2,9-dione

Guidance literature:: With triethylamine; In toluene; Ambient temperature;
DOI:10.1002/hlca.19910740402

Reference yield:

: 51673-59-7
1-(2-nitrophenyl)ethane-1,2-diol

: 135949-42-7
5-(2-nitrophenyl)-4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo<8.8.8>hexacosane-2,9-dione

Guidance literature:: Multi-step reaction with 4 steps

1: 59 percent / NaH / tetrahydrofuran / 12 h / Ambient temperature

2: 82 percent / CF₃CO₂H / 0.5 h / Ambient temperature

3: 90 percent / oxalyl chloride / toluene / 20 h / Ambient temperature

4: 75 percent / Et₃N / toluene / Ambient temperature

With oxalyl dichloride; sodium hydride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; toluene;
DOI:10.1002/hlca.19910740402

Reference yield:

: 135949-36-9
4-(2-nitrophenyl)-3,6-dioxaoctanedioic acid

: 135949-42-7
5-(2-nitrophenyl)-4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo<8.8.8>hexacosane-2,9-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / oxalyl chloride / toluene / 20 h / Ambient temperature

2: 75 percent / Et₃N / toluene / Ambient temperature

With oxalyl dichloride; triethylamine; In toluene;
DOI:10.1002/hlca.19910740402