C₂₄H₂₈N₂O₅

Base Information

Chemical Name:C₂₄H₂₈N₂O₅
CAS No.:1390618-82-2
Molecular Formula:C₂₄H₂₈N₂O₅
Molecular Weight:424.497
Hs Code.:

C<sub>24</sub>H<sub>28</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₄H₂₈N₂O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₂₈N₂O₅

Chemical Property:

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Technology Process of C₂₄H₂₈N₂O₅

There total 5 articles about C₂₄H₂₈N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1390618-56-0
C₂₃H₂₆N₂O₅

: 74-88-4
methyl iodide

: 1390618-82-2
C₂₄H₂₈N₂O₅

Guidance literature:: C₂₃H₂₆N₂O₅; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 62-53-3
aniline

: 1390618-82-2
C₂₄H₂₈N₂O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium phosphate / acetonitrile / 1 h / 0 - 20 °C

2.1: ammonia / water; acetonitrile / 40 °C

3.1: caesium carbonate / (3,5-dioxa-4-phospha-cyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-dimethyl-amine; copper(I) bromide / N,N-dimethyl-formamide / 100 °C / Inert atmosphere

4.1: dmap / acetonitrile / 12 h / 20 °C

5.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

5.2: 20 °C

With potassium phosphate; ammonia; caesium carbonate; lithium diisopropyl amide; dmap; (3,5-dioxa-4-phospha-cyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-dimethyl-amine; copper(I) bromide; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 77868-83-8
(+/-)-3-bromo-1-phenyl-2-pyrrolidinone

: 1390618-82-2
C₂₄H₂₈N₂O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: ammonia / water; acetonitrile / 40 °C

2.1: caesium carbonate / (3,5-dioxa-4-phospha-cyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-dimethyl-amine; copper(I) bromide / N,N-dimethyl-formamide / 100 °C / Inert atmosphere

3.1: dmap / acetonitrile / 12 h / 20 °C

4.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

4.2: 20 °C

With ammonia; caesium carbonate; lithium diisopropyl amide; dmap; (3,5-dioxa-4-phospha-cyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-dimethyl-amine; copper(I) bromide; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile;