2-[(4-methoxyphenyl)methyl]phenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Base Information

Chemical Name:2-[(4-methoxyphenyl)methyl]phenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside
CAS No.:360775-87-7
Molecular Formula:C₂₈H₃₂O₁₁
Molecular Weight:544.555
Hs Code.:

Synonyms:2-[(4-methoxyphenyl)methyl]phenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[(4-methoxyphenyl)methyl]phenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

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Technology Process of 2-[(4-methoxyphenyl)methyl]phenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

There total 13 articles about 2-[(4-methoxyphenyl)methyl]phenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 37155-50-3
2-(4-methoxybenzyl)phenol

: 604-69-3
β-D-glucose pentaacetate

: 360775-87-7
2-[(4-methoxyphenyl)methyl]phenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; triethylamine; In toluene; at 40 ℃; for 6h; Temperature; Solvent;
DOI:10.3987/COM-16-13484

Reference yield: 90.0%

: 37155-50-3
2-(4-methoxybenzyl)phenol

: 92052-29-4
2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl trichloroacetimidate

: 360775-87-7
2-[(4-methoxyphenyl)methyl]phenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In ethyl acetate; for 2h;
DOI:10.3987/COM-16-13484

Reference yield: 53.0%

: 37155-50-3
2-(4-methoxybenzyl)phenol

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 360775-87-7
2-[(4-methoxyphenyl)methyl]phenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: 2-(4-methoxybenzyl)phenol; With tetrabutylammomium bromide; sodium hydroxide; In dichloromethane; water; at 0 ℃; for 0.25h;

2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide; In dichloromethane; water; at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2016.03.065