tert-butyl isopropyl(5-(8-phenylimidazo[1,2-a]pyrazin-6-yl)thiazol-5-yl)carbamate

Base Information

Chemical Name:tert-butyl isopropyl(5-(8-phenylimidazo[1,2-a]pyrazin-6-yl)thiazol-5-yl)carbamate
CAS No.:1202278-30-5
Molecular Formula:C₂₃H₂₅N₅O₂S
Molecular Weight:435.55
Hs Code.:

Synonyms:tert-butyl isopropyl(5-(8-phenylimidazo[1,2-a]pyrazin-6-yl)thiazol-5-yl)carbamate

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Chemical Property of tert-butyl isopropyl(5-(8-phenylimidazo[1,2-a]pyrazin-6-yl)thiazol-5-yl)carbamate

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Technology Process of tert-butyl isopropyl(5-(8-phenylimidazo[1,2-a]pyrazin-6-yl)thiazol-5-yl)carbamate

There total 6 articles about tert-butyl isopropyl(5-(8-phenylimidazo[1,2-a]pyrazin-6-yl)thiazol-5-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107-20-0
2-chloroethanal

: 1202278-29-2
tert-butyl 5-(5-amino-6-phenylpyrazin-2-yl)thiazol-2-yl(isopropyl)carbamate

: 1202278-30-5
tert-butyl isopropyl(5-(8-phenylimidazo[1,2-a]pyrazin-6-yl)thiazol-5-yl)carbamate

Guidance literature:: In ethanol; at 60 ℃; for 24h;

Reference yield:

: 170961-15-6
tert-butyl 1,3-thiazole-2-yl-carbamate

: 1202278-30-5
tert-butyl isopropyl(5-(8-phenylimidazo[1,2-a]pyrazin-6-yl)thiazol-5-yl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / -20 - 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / 2 h / -78 °C

2.2: -78 - 20 °C

3.1: N-ethyl-N,N-diisopropylamine / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 18 h / 85 °C

4.1: ethanol / 24 h / 60 °C

With N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium diisopropyl amide; diethylazodicarboxylate; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 344940-70-1
5-bromo-3-phenyl-pyrazin-2-amine

: 1202278-30-5
tert-butyl isopropyl(5-(8-phenylimidazo[1,2-a]pyrazin-6-yl)thiazol-5-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 18 h / 85 °C

2: ethanol / 24 h / 60 °C

With N-ethyl-N,N-diisopropylamine; bis-triphenylphosphine-palladium(II) chloride; In ethanol; N,N-dimethyl-formamide;