N'-(2,6-dichlorobenzylidene)-4-methylbenzene-1-sulfonohydrazide

Base Information

• Chemical Name: N'-(2,6-dichlorobenzylidene)-4-methylbenzene-1-sulfonohydrazide
• CAS No.: 37532-04-0
• Molecular Formula: C₁₄H₁₂Cl₂N₂O₂S
• Molecular Weight: 343.233
• Mol file: 37532-04-0.mol

Synonyms:N'-(2,6-dichlorobenzylidene)-4-methylbenzene-1-sulfonohydrazide

Chemical Property of N'-(2,6-dichlorobenzylidene)-4-methylbenzene-1-sulfonohydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N'-(2,6-dichlorobenzylidene)-4-methylbenzene-1-sulfonohydrazide

There total 1 articles about N'-(2,6-dichlorobenzylidene)-4-methylbenzene-1-sulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2,6-dichlorobenzaldehyde (83-38-5) + toluene-4-sulfonic acid hydrazide (1576-35-8) → N'-(2,6-dichlorobenzylidene)-4-methylbenzene-1-sulfonohydrazide (37532-04-0)

Guidance literature:

In methanol; at 20 ℃; for 2h;

DOI:10.1021/jo202598e

Reference yield: 94.0%

N'-(2,6-dichlorobenzylidene)-4-methylbenzene-1-sulfonohydrazide (37532-04-0) → 2,6-dichlorobenzoic acid (50-30-6)

Guidance literature:

With poly(diselanediyl-1,2-phenylene); dihydrogen peroxide; In tetrahydrofuran; for 144h; Heating;

DOI:10.1081/SCC-100105891

Reference yield: 93.0%

N'-(2,6-dichlorobenzylidene)-4-methylbenzene-1-sulfonohydrazide (37532-04-0) → 2,6-dichlorophenyl (O,1-(2)H2)methanol (1400741-60-7)

Guidance literature:

With water-d2; potassium carbonate; at 130 ℃; for 0.5h; Microwave irradiation;

DOI:10.1055/s-0031-1290372

upstream raw materials:

2,6-dichlorobenzaldehyde

toluene-4-sulfonic acid hydrazide

Downstream raw materials:

2,6-dichlorobenzoic acid

2,6-dichlorobenzaldehyde

3-(2,6-dichlorophenyl)-1H-indazole

2,6-dichlorobenzaldehyde (2,6-dichlorobenzylidene)hydrazone