N-(4-(N¹-methyl-N²-methyl-N²-(methyloxy)oxalamido)benzyl)adamantanecarboxamide

Base Information

Chemical Name:N-(4-(N¹-methyl-N²-methyl-N²-(methyloxy)oxalamido)benzyl)adamantanecarboxamide
CAS No.:1542915-44-5
Molecular Formula:C₂₃H₃₁N₃O₄
Molecular Weight:413.517
Hs Code.:

N-(4-(N<SUP>1</SUP>-methyl-N<SUP>2</SUP>-methyl-N<SUP>2</SUP>-(methyloxy)oxalamido)benzyl)adamantanecarboxamide

Synonyms:N-(4-(N¹-methyl-N²-methyl-N²-(methyloxy)oxalamido)benzyl)adamantanecarboxamide

Suppliers and Price of N-(4-(N¹-methyl-N²-methyl-N²-(methyloxy)oxalamido)benzyl)adamantanecarboxamide

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Chemical Property of N-(4-(N¹-methyl-N²-methyl-N²-(methyloxy)oxalamido)benzyl)adamantanecarboxamide

Chemical Property:

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Technology Process of N-(4-(N¹-methyl-N²-methyl-N²-(methyloxy)oxalamido)benzyl)adamantanecarboxamide

There total 6 articles about N-(4-(N¹-methyl-N²-methyl-N²-(methyloxy)oxalamido)benzyl)adamantanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4403-71-8
(4-aminomethyl)aniline

: 1542915-44-5
N-(4-(N¹-methyl-N²-methyl-N²-(methyloxy)oxalamido)benzyl)adamantanecarboxamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: dmap / dichloromethane / 0.17 h / 20 °C

1.2: 20 °C

2.1: triethylamine / dichloromethane / 0 - 20 °C

3.1: water; sodium hydroxide / ethanol / 20 °C

4.1: dmap; triethylamine / dichloromethane / 0.17 h / 20 °C

4.2: 20 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With dmap; water; potassium carbonate; triethylamine; sodium hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2013.12.027

Reference yield:

: 1542915-40-1
N-(4-(N²-methyl-N²-(methyloxy)oxalamido)benzyl)adamantanecarboxamide

: 74-88-4
methyl iodide

: 1542915-44-5
N-(4-(N¹-methyl-N²-methyl-N²-(methyloxy)oxalamido)benzyl)adamantanecarboxamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.bmc.2013.12.027

Reference yield:

: C₂₀H₂₄N₂O₄

: 1542915-44-5
N-(4-(N¹-methyl-N²-methyl-N²-(methyloxy)oxalamido)benzyl)adamantanecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap; triethylamine / dichloromethane / 0.17 h / 20 °C

1.2: 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With dmap; potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2013.12.027