Technology Process of C25H26N4O3
There total 6 articles about C25H26N4O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium diacetate; sodium carbonate; ruphos;
at 100 ℃;
for 22h;
Inert atmosphere;
Microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 2 h / 20 °C
1.2: 2 h / 25 - 40 °C / Cooling with ice
2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -30 - -10 °C / Inert atmosphere
2.2: 2 h / -30 - -10 °C / Inert atmosphere
2.3: 10.5 h / 20 °C
3.1: diethylamine / N,N-dimethyl-formamide / 20 °C
4.1: sodium carbonate; palladium diacetate; ruphos / 22 h / 100 °C / Inert atmosphere; Microwave irradiation
With
n-butyllithium; oxalyl dichloride; palladium diacetate; sodium carbonate; diethylamine; ruphos;
In
tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -30 - -10 °C / Inert atmosphere
1.2: 2 h / -30 - -10 °C / Inert atmosphere
1.3: 10.5 h / 20 °C
2.1: diethylamine / N,N-dimethyl-formamide / 20 °C
3.1: sodium carbonate; palladium diacetate; ruphos / 22 h / 100 °C / Inert atmosphere; Microwave irradiation
With
n-butyllithium; palladium diacetate; sodium carbonate; diethylamine; ruphos;
In
tetrahydrofuran; hexane; N,N-dimethyl-formamide;