[(2R)-2-methyl-3-(phenylmethoxy)-1-propyl][1-amino-2-phenylethyl]diphenylsilane

Base Information

Chemical Name:[(2R)-2-methyl-3-(phenylmethoxy)-1-propyl][1-amino-2-phenylethyl]diphenylsilane
CAS No.:849773-85-9
Molecular Formula:C₃₁H₃₅NOSi
Molecular Weight:465.71
Hs Code.:

Synonyms:[(2R)-2-methyl-3-(phenylmethoxy)-1-propyl][1-amino-2-phenylethyl]diphenylsilane

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Chemical Property of [(2R)-2-methyl-3-(phenylmethoxy)-1-propyl][1-amino-2-phenylethyl]diphenylsilane

Chemical Property:

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Technology Process of [(2R)-2-methyl-3-(phenylmethoxy)-1-propyl][1-amino-2-phenylethyl]diphenylsilane

There total 11 articles about [(2R)-2-methyl-3-(phenylmethoxy)-1-propyl][1-amino-2-phenylethyl]diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 727726-44-5
2-[[1-[(2R)-2-methyl-3-(phenylmethoxy)-1-propyl]diphenylsilyl]-2-phenylethyl]-1H-isoindole-1,3(2H)-dione

: 849773-85-9
[(2R)-2-methyl-3-(phenylmethoxy)-1-propyl][1-amino-2-phenylethyl]diphenylsilane

Guidance literature:: With hydrazine; In ethanol; Heating;
DOI:10.1016/j.bmcl.2004.03.042

Reference yield:

: 63930-46-1
(S)-3-benzyloxy-2-methylpropan-1-ol

: 849773-85-9
[(2R)-2-methyl-3-(phenylmethoxy)-1-propyl][1-amino-2-phenylethyl]diphenylsilane

Guidance literature:: Multi-step reaction with 6 steps

1.1: 85 percent / iodine; triphenylphosphine; imidazole / diethyl ether; acetonitrile / 3.5 h / 0 °C

2.1: tert-butyllithium / pentane; diethyl ether / 0.83 h / -78 - 20 °C

2.2: 65 percent / diethyl ether; pentane / -78 - 20 °C

3.1: 73 percent / HgCl₂; water / acetonitrile / 1.25 h / 20 °C

4.1: 100 percent / LiAlH₄ / diethyl ether / 3 h / 0 - 20 °C

5.1: 63 percent / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran / 24 h / 20 °C

6.1: hydrazine / ethanol / 6 h / Heating

With 1H-imidazole; lithium aluminium tetrahydride; water; iodine; tert.-butyl lithium; triphenylphosphine; mercury dichloride; hydrazine; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; ethanol; acetonitrile; pentane;
DOI:10.1021/jo048121v

Reference yield:

: 81927-55-1
O-benzyl 2,2,2-trichloroacetimidate

: 849773-85-9
[(2R)-2-methyl-3-(phenylmethoxy)-1-propyl][1-amino-2-phenylethyl]diphenylsilane

Guidance literature:: Multi-step reaction with 8 steps

1.1: TfOH

2.1: lithium aluminum hydride

3.1: 85 percent / iodine; triphenylphosphine; imidazole / diethyl ether; acetonitrile / 3.5 h / 0 °C

4.1: tert-butyllithium / pentane; diethyl ether / 0.83 h / -78 - 20 °C

4.2: 65 percent / diethyl ether; pentane / -78 - 20 °C

5.1: 73 percent / HgCl₂; water / acetonitrile / 1.25 h / 20 °C

6.1: 100 percent / LiAlH₄ / diethyl ether / 3 h / 0 - 20 °C

7.1: 63 percent / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran / 24 h / 20 °C

8.1: hydrazine / ethanol / 6 h / Heating

With 1H-imidazole; lithium aluminium tetrahydride; trifluorormethanesulfonic acid; water; iodine; tert.-butyl lithium; triphenylphosphine; mercury dichloride; hydrazine; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; ethanol; acetonitrile; pentane;
DOI:10.1021/jo048121v