N-Benzyloxycarbonyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-N'-Succinimidoyl Ester

Base Information

• Chemical Name: N-Benzyloxycarbonyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-N'-Succinimidoyl Ester
• CAS No.: 64153-37-3
• Molecular Formula: C₂₆H₃₄N₂O₁₀
• Molecular Weight: 534.563

Synonyms:N-Benzyloxycarbonyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-N'-Succinimidoyl Ester

Chemical Property of N-Benzyloxycarbonyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-N'-Succinimidoyl Ester

Chemical Property:

Purity/Quality:

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Technology Process of N-Benzyloxycarbonyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-N'-Succinimidoyl Ester

There total 2 articles about N-Benzyloxycarbonyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-N'-Succinimidoyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-hydroxy-pyrrolidine-2,5-dione (6066-82-6) + N-(benzyloxycarbonyl)-γ,γ-di-tert-butyl-L-γ-carboxyglutamic acid (60686-50-2,60686-52-4) → N-Benzyloxycarbonyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-N'-Succinimidoyl Ester (64153-37-3)

Guidance literature:

With dicyclohexyl-carbodiimide; In ethyl acetate; 1.) 0 deg C, 2 h, 2.) RT, overnight;

DOI:10.1021/jo00170a015

Reference yield:

→ N-Benzyloxycarbonyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-N'-Succinimidoyl Ester (64153-37-3)

Guidance literature:

/BRN= 193035/, N-Hydroxysuccinimid;

DOI:10.1002/hlca.19770600311

Reference yield: 85.0%

L-arginine (74-79-3,25212-18-4) + N-Benzyloxycarbonyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-N'-Succinimidoyl Ester (64153-37-3) → N-Benzyloxycarbonyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamyl-L-arginine (87136-42-3)

Guidance literature:

With 4-methyl-morpholine; trifluoroacetic acid; In N,N-dimethyl-formamide; for 48h; Ambient temperature;

DOI:10.1021/jo00170a015

upstream raw materials:

1-hydroxy-pyrrolidine-2,5-dione

N-(benzyloxycarbonyl)-γ,γ-di-tert-butyl-L-γ-carboxyglutamic acid

Downstream raw materials:

N-Benzyloxycarbonyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamyl-L-arginine

N-Benzyloxycarbonyl-L-γ-carboxyglutamyl-L-arginyl-L-γ-carboxyglutamic Acid α-Methyl Ester Trifluoroacetate Salt

γ,γ-Di-tert-butyl-L-γ-carboxyglutamyl-L-arginyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-Methyl Ester p-Toluenesulfonate Salt

N-Benzyloxycarbonyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamyl-L-arginyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-Methyl Ester Acetate Salt

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