(E)-5'-amino-N₆-tert-butoxycarbonyl-5'-deoxy-5'-N-{[3-(2-methoxymethoxy)phenyl]prop-2-ene-1-oyl}-2',3'-O-isopropylideneadenosine

Base Information

• Chemical Name: (E)-5'-amino-N₆-tert-butoxycarbonyl-5'-deoxy-5'-N-{[3-(2-methoxymethoxy)phenyl]prop-2-ene-1-oyl}-2',3'-O-isopropylideneadenosine
• CAS No.: 939794-46-4
• Molecular Formula: C₂₉H₃₆N₆O₈
• Molecular Weight: 596.64

Synonyms:(E)-5'-amino-N₆-tert-butoxycarbonyl-5'-deoxy-5'-N-{[3-(2-methoxymethoxy)phenyl]prop-2-ene-1-oyl}-2',3'-O-isopropylideneadenosine

Chemical Property of (E)-5'-amino-N₆-tert-butoxycarbonyl-5'-deoxy-5'-N-{[3-(2-methoxymethoxy)phenyl]prop-2-ene-1-oyl}-2',3'-O-isopropylideneadenosine

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Technology Process of (E)-5'-amino-N₆-tert-butoxycarbonyl-5'-deoxy-5'-N-{[3-(2-methoxymethoxy)phenyl]prop-2-ene-1-oyl}-2',3'-O-isopropylideneadenosine

There total 1 articles about (E)-5'-amino-N₆-tert-butoxycarbonyl-5'-deoxy-5'-N-{[3-(2-methoxymethoxy)phenyl]prop-2-ene-1-oyl}-2',3'-O-isopropylideneadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

tert-butyl 9-(((3aR,4R,6R,6aR)-6-(aminomethyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-yl)carbamate (873556-45-7) + (E)-[3-(2-methoxymethoxy)phenyl]prop-2ene-1-oic acid (310391-27-6) → (E)-5'-amino-N6-tert-butoxycarbonyl-5'-deoxy-5'-N-{[3-(2-methoxymethoxy)phenyl]prop-2-ene-1-oyl}-2',3'-O-isopropylideneadenosine (939794-46-4)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; for 16h;

Reference yield: 87.0%

(E)-5'-amino-N6-tert-butoxycarbonyl-5'-deoxy-5'-N-{[3-(2-methoxymethoxy)phenyl]prop-2-ene-1-oyl}-2',3'-O-isopropylideneadenosine (939794-46-4) → (E)-5'-amino-5'-deoxy-5'-N-{[3-(2-hydroxy)phenyl]prop-2-ene-1-oyl}adenosine (939793-78-9)

Guidance literature:

With trifluoroacetic acid; In water; at 0 ℃; for 0.5h;

upstream raw materials:

tert-butyl 9-(((3aR,4R,6R,6aR)-6-(aminomethyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-yl)carbamate

(E)-[3-(2-methoxymethoxy)phenyl]prop-2ene-1-oic acid

Downstream raw materials:

(E)-5'-amino-5'-deoxy-5'-N-{[3-(2-hydroxy)phenyl]prop-2-ene-1-oyl}adenosine

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