(η5-cyclopentadienyl)Fe(CO)2(CH2CH=C(CH3)2)

Base Information

Chemical Name:(η5-cyclopentadienyl)Fe(CO)2(CH2CH=C(CH3)2)
CAS No.:38905-70-3
Molecular Formula:C₁₂H₁₄FeO₂
Molecular Weight:246.089
Hs Code.:

Synonyms:(η5-cyclopentadienyl)Fe(CO)2(CH2CH=C(CH3)2)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (η5-cyclopentadienyl)Fe(CO)2(CH2CH=C(CH3)2)

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Technology Process of (η5-cyclopentadienyl)Fe(CO)2(CH2CH=C(CH3)2)

There total 3 articles about (η5-cyclopentadienyl)Fe(CO)2(CH2CH=C(CH3)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 35913-82-7
cyclopentadienylirondicarbonyl hydride

: 78-79-5,9003-31-0
isoprene

: 513-35-9
2-methyl-but-2-ene

: 38117-54-3
cyclopentadienyl iron(II) dicarbonyl dimer

: 38905-70-3
(η5-cyclopentadienyl)Fe(CO)2(CH2CH=C(CH3)2)

: 563-46-2
2-Methyl-1-butene

: 563-45-1
3-Methyl-1-butene

Guidance literature:: In pentane; under N2, stirring at room temp, the react. was complete within 20-30 min; evapn. (vac.), chromy. on alumina (eluent pentane for the hydrometalated products, and more polar solvents for the dimer), the org. products identiefied by GC and NMR;

Reference yield:

: 35913-82-7
cyclopentadienylirondicarbonyl hydride

: 78-79-5,9003-31-0
isoprene

: 513-35-9
2-methyl-but-2-ene

: 38905-70-3
(η5-cyclopentadienyl)Fe(CO)2(CH2CH=C(CH3)2)

: 563-45-1
3-Methyl-1-butene

Guidance literature:: In benzene-d6; under N2 for 7-10 min (molar ratio metal hydride:diene = ca. 2:1);; detected by CIDNP studies;;
DOI:10.1039/c39860000312

Reference yield:

: 35913-82-7
cyclopentadienylirondicarbonyl hydride

: 78-79-5,9003-31-0
isoprene

: 38117-54-3
cyclopentadienyl iron(II) dicarbonyl dimer

: 38905-70-3
(η5-cyclopentadienyl)Fe(CO)2(CH2CH=C(CH3)2)

Guidance literature:: With thiophenol; In pentane; under N2, stirring at room temp, the react. was complete in <1 h; evapn. (vac.), chromy. on alumina (eluent pentane for the hydrometalated products, and more polar solvents for the dimer);