N-(4-(2-(2H-tetrazol-5-yl)ethyl)-5-thioxo-4,5-dihydro-1,3,4-thiadiazol-2-yl)benzamide

Base Information

Chemical Name:N-(4-(2-(2H-tetrazol-5-yl)ethyl)-5-thioxo-4,5-dihydro-1,3,4-thiadiazol-2-yl)benzamide
CAS No.:1356861-62-5
Molecular Formula:C₁₂H₁₁N₇OS₂
Molecular Weight:333.398
Hs Code.:

Synonyms:N-(4-(2-(2H-tetrazol-5-yl)ethyl)-5-thioxo-4,5-dihydro-1,3,4-thiadiazol-2-yl)benzamide

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Chemical Property of N-(4-(2-(2H-tetrazol-5-yl)ethyl)-5-thioxo-4,5-dihydro-1,3,4-thiadiazol-2-yl)benzamide

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Technology Process of N-(4-(2-(2H-tetrazol-5-yl)ethyl)-5-thioxo-4,5-dihydro-1,3,4-thiadiazol-2-yl)benzamide

There total 3 articles about N-(4-(2-(2H-tetrazol-5-yl)ethyl)-5-thioxo-4,5-dihydro-1,3,4-thiadiazol-2-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1356861-61-4
N-(4-(2-cyanoethyl)-5-thioxo-4,5-dihydro-1,3,4-thiadiazol-2-yl)benzamide

: 1356861-62-5
N-(4-(2-(2H-tetrazol-5-yl)ethyl)-5-thioxo-4,5-dihydro-1,3,4-thiadiazol-2-yl)benzamide

Guidance literature:: With sodium azide; ammonium chloride; In N,N-dimethyl-formamide; at 120 ℃; for 6h;
DOI:10.5012/bkcs.2011.32.12.4227

Reference yield:

: 98-88-4
benzoyl chloride

: 1356861-62-5
N-(4-(2-(2H-tetrazol-5-yl)ethyl)-5-thioxo-4,5-dihydro-1,3,4-thiadiazol-2-yl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / N,N-dimethyl-formamide / 8 h / 20 °C

2: triethylamine / ethanol / 6 h / Reflux

3: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 6 h / 120 °C

With sodium azide; ammonium chloride; triethylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.5012/bkcs.2011.32.12.4227

Reference yield:

: 33949-86-9
N-(5-mercapto-1,3,4-thiadiazol-2-yl)benzamide

: 1356861-62-5
N-(4-(2-(2H-tetrazol-5-yl)ethyl)-5-thioxo-4,5-dihydro-1,3,4-thiadiazol-2-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / ethanol / 6 h / Reflux

2: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 6 h / 120 °C

With sodium azide; ammonium chloride; triethylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.5012/bkcs.2011.32.12.4227