acetic acid 5-hydroxy-1-[1-(4-methoxy-benzyl)-1H-indol-2-yl]-hexyl ester

Base Information

Chemical Name:acetic acid 5-hydroxy-1-[1-(4-methoxy-benzyl)-1H-indol-2-yl]-hexyl ester
CAS No.:1360148-50-0
Molecular Formula:C₂₄H₂₉NO₄
Molecular Weight:395.499
Hs Code.:

Synonyms:acetic acid 5-hydroxy-1-[1-(4-methoxy-benzyl)-1H-indol-2-yl]-hexyl ester

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Chemical Property of acetic acid 5-hydroxy-1-[1-(4-methoxy-benzyl)-1H-indol-2-yl]-hexyl ester

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Technology Process of acetic acid 5-hydroxy-1-[1-(4-methoxy-benzyl)-1H-indol-2-yl]-hexyl ester

There total 10 articles about acetic acid 5-hydroxy-1-[1-(4-methoxy-benzyl)-1H-indol-2-yl]-hexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1360148-48-6
acetic acid 1-[1-(4-methoxy-benzyl)-1H-indol-2-yl]-5-oxopentyl ester

: 75-16-1
methylmagnesium bromide

: 1360148-50-0
acetic acid 5-hydroxy-1-[1-(4-methoxy-benzyl)-1H-indol-2-yl]-hexyl ester

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃; for 3h;
DOI:10.5012/bkcs.2011.32.12.4309

Reference yield: 50.0%

: 1360148-44-2
acetic acid 1-[1-(4-methoxy-benzyl)-1H-indol-2-yl]-hex-5-enyl ester

: 1360148-50-0
acetic acid 5-hydroxy-1-[1-(4-methoxy-benzyl)-1H-indol-2-yl]-hexyl ester

Guidance literature:: acetic acid 1-[1-(4-methoxy-benzyl)-1H-indol-2-yl]-hex-5-enyl ester; With mercury(II) diacetate; In tetrahydrofuran; water; at 20 ℃; for 2h;

With sodium tetrahydroborate; sodium hydroxide; In tetrahydrofuran; water;
DOI:10.5012/bkcs.2011.32.12.4309

Reference yield:

: 161466-19-9
1-(4-methoxy-benzyl)-1H-indole-2-carboxylic acid ethyl ester

: 1360148-50-0
acetic acid 5-hydroxy-1-[1-(4-methoxy-benzyl)-1H-indol-2-yl]-hexyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C

2.1: manganese(IV) oxide / tetrachloromethane / 10 h / 20 °C

3.1: magnesium / diethyl ether / 2 h / 20 °C

3.2: 0 °C

4.1: dmap / dichloromethane / 5 h / 20 °C

5.1: mercury(II) diacetate / tetrahydrofuran; water / 2 h / 20 °C

With dmap; manganese(IV) oxide; lithium aluminium tetrahydride; mercury(II) diacetate; magnesium; In tetrahydrofuran; tetrachloromethane; diethyl ether; dichloromethane; water; 3.2: Grignard reaction;
DOI:10.5012/bkcs.2011.32.12.4309