5-benzoyloxy-2(E),4(E)-pentadienoyl azide

Base Information

Chemical Name:5-benzoyloxy-2(E),4(E)-pentadienoyl azide
CAS No.:84525-45-1
Molecular Formula:C₁₂H₉N₃O₃
Molecular Weight:243.222
Hs Code.:

Synonyms:5-benzoyloxy-2(E),4(E)-pentadienoyl azide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-benzoyloxy-2(E),4(E)-pentadienoyl azide

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Technology Process of 5-benzoyloxy-2(E),4(E)-pentadienoyl azide

There total 3 articles about 5-benzoyloxy-2(E),4(E)-pentadienoyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 84525-44-0
5-benzoyloxy-2(E),4(E)-pentadienoyl chloride

: 84525-45-1
5-benzoyloxy-2(E),4(E)-pentadienoyl azide

Guidance literature:: With trimethylsilylazide; In dichloromethane; at 0 ℃; for 30h;
DOI:10.1055/s-1982-30020

Reference yield:

: 24338-67-8
4-benzoyloxy-trans-2-trans-4-pentadienal

: 84525-45-1
5-benzoyloxy-2(E),4(E)-pentadienoyl azide

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / resorcinol, sodium chlorite / ethanol / 24 h / Ambient temperature; buffer (aq. solution citric acid and trisodium salt citric acid) - pH=3,6

2: thionyl chloride, hydroquinone / 2 h / 50 °C

3: 78 percent / azidotrimethylsilane / CH₂Cl₂ / 30 h / 0 °C

With sodium chlorite; thionyl chloride; trimethylsilylazide; hydroquinone; recorcinol; In ethanol; dichloromethane;
DOI:10.1055/s-1982-30020

Reference yield:

: 84541-23-1
5-benzoyloxy-2(E),4(E)-pentadienoic acid

: 84525-45-1
5-benzoyloxy-2(E),4(E)-pentadienoyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride, hydroquinone / 2 h / 50 °C

2: 78 percent / azidotrimethylsilane / CH₂Cl₂ / 30 h / 0 °C

With thionyl chloride; trimethylsilylazide; hydroquinone; In dichloromethane;
DOI:10.1055/s-1982-30020