N₂-acetoacetyl-2 hydroxybenzohydrazide

Base Information

• Chemical Name: N₂-acetoacetyl-2 hydroxybenzohydrazide
• CAS No.: 401936-08-1
• Molecular Formula: C₁₁H₁₂N₂O₄
• Molecular Weight: 236.227
• Mol file: 401936-08-1.mol

Synonyms:N₂-acetoacetyl-2 hydroxybenzohydrazide

Chemical Property of N₂-acetoacetyl-2 hydroxybenzohydrazide

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

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Technology Process of N₂-acetoacetyl-2 hydroxybenzohydrazide

There total 1 articles about N₂-acetoacetyl-2 hydroxybenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl acetoacetate (141-97-9) + 2-Hydroxybenzoylhydrazine (936-02-7) → N2-acetoacetyl-2 hydroxybenzohydrazide (401936-08-1)

Guidance literature:

at 150 ℃; for 1h;

DOI:10.1007/s00044-010-9532-x

Reference yield: 70.0%

N2-acetoacetyl-2 hydroxybenzohydrazide (401936-08-1) + 3,4,5-trimethoxy-benzaldehyde (86-81-7) + thiourea (17356-08-0) → C22H24N4O6S (1325237-27-1)

Guidance literature:

With hydrogenchloride; In ethanol; water; at 20 ℃; Reflux;

DOI:10.1007/s00044-010-9532-x

Reference yield: 68.0%

N2-acetoacetyl-2 hydroxybenzohydrazide (401936-08-1) + 3-nitro-benzaldehyde (99-61-6) + urea (57-13-6) → C19H17N5O6 (1325237-25-9)

Guidance literature:

With hydrogenchloride; In ethanol; water; at 20 ℃; Reflux;

DOI:10.1007/s00044-010-9532-x

upstream raw materials:

ethyl acetoacetate

2-Hydroxybenzoylhydrazine

Downstream raw materials:

C₁₉H₁₇N₅O₅S

C₁₉H₁₇N₅O₆

C₂₂H₂₄N₄O₆S

C₂₁H₂₃N₅O₃S