2-(N-(2-methoxybenzyl)-N-[2-(N,N-dimethyl)aminoethyl]aminomethyl)-4,6-dichlorophenol

Base Information

Chemical Name:2-(N-(2-methoxybenzyl)-N-[2-(N,N-dimethyl)aminoethyl]aminomethyl)-4,6-dichlorophenol
CAS No.:1227408-27-6
Molecular Formula:C₁₉H₂₄Cl₂N₂O₂
Molecular Weight:383.318
Hs Code.:

Synonyms:2-(N-(2-methoxybenzyl)-N-[2-(N,N-dimethyl)aminoethyl]aminomethyl)-4,6-dichlorophenol

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Chemical Property of 2-(N-(2-methoxybenzyl)-N-[2-(N,N-dimethyl)aminoethyl]aminomethyl)-4,6-dichlorophenol

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Technology Process of 2-(N-(2-methoxybenzyl)-N-[2-(N,N-dimethyl)aminoethyl]aminomethyl)-4,6-dichlorophenol

There total 3 articles about 2-(N-(2-methoxybenzyl)-N-[2-(N,N-dimethyl)aminoethyl]aminomethyl)-4,6-dichlorophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: OCH₃C₆H₄CHNCH₂CH₂N(CH₃)2

: 1227408-27-6
2-(N-(2-methoxybenzyl)-N-[2-(N,N-dimethyl)aminoethyl]aminomethyl)-4,6-dichlorophenol

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 12 h / 0 °C / Inert atmosphere

2: methanol / 12 h / 80 °C / Inert atmosphere

With sodium tetrahydroborate; In methanol; 2: Mannich reaction;
DOI:10.1039/c0dt00250j

Reference yield:

: 135-02-4
ortho-anisaldehyde

: 1227408-27-6
2-(N-(2-methoxybenzyl)-N-[2-(N,N-dimethyl)aminoethyl]aminomethyl)-4,6-dichlorophenol

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 24 h / Inert atmosphere; Reflux

2: sodium tetrahydroborate / methanol / 12 h / 0 °C / Inert atmosphere

3: methanol / 12 h / 80 °C / Inert atmosphere

With sodium tetrahydroborate; In methanol; 3: Mannich reaction;
DOI:10.1039/c0dt00250j