5-(1,2-dithiolan-3-yl)-N-(1-(3-methoxybenzyl)piperidin-4-yl)pentanamide

Base Information

Chemical Name:5-(1,2-dithiolan-3-yl)-N-(1-(3-methoxybenzyl)piperidin-4-yl)pentanamide
CAS No.:1294304-18-9
Molecular Formula:C₂₁H₃₂N₂O₂S₂
Molecular Weight:408.629
Hs Code.:

Synonyms:5-(1,2-dithiolan-3-yl)-N-(1-(3-methoxybenzyl)piperidin-4-yl)pentanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(1,2-dithiolan-3-yl)-N-(1-(3-methoxybenzyl)piperidin-4-yl)pentanamide

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Technology Process of 5-(1,2-dithiolan-3-yl)-N-(1-(3-methoxybenzyl)piperidin-4-yl)pentanamide

There total 6 articles about 5-(1,2-dithiolan-3-yl)-N-(1-(3-methoxybenzyl)piperidin-4-yl)pentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1-(3-methoxybenzyl)piperidin-4-amine trifluoroacetic acid

: 1077-28-7,62-46-4
Thioctic acid

: 1294304-18-9
5-(1,2-dithiolan-3-yl)-N-(1-(3-methoxybenzyl)piperidin-4-yl)pentanamide

Guidance literature:: With triethylamine; In dichloromethane;

Reference yield:

: 1-(3-methoxybenzyl)piperidin-4-amine trifluoroacetic acid

: 40846-94-4
thioctic acid-N-hydroxysuccinimide ester

: 1294304-18-9
5-(1,2-dithiolan-3-yl)-N-(1-(3-methoxybenzyl)piperidin-4-yl)pentanamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.5012/bkcs.2014.35.6.1681

Reference yield:

: 73874-95-0
(piperidin-4-yl)carbamic acid tert-butyl ester

: 1294304-18-9
5-(1,2-dithiolan-3-yl)-N-(1-(3-methoxybenzyl)piperidin-4-yl)pentanamide

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine; triethylamine / dichloromethane / Inert atmosphere

2: dichloromethane / Inert atmosphere

3: triethylamine / dichloromethane / 5 h / 20 °C / Inert atmosphere

With triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.5012/bkcs.2014.35.6.1681