diisopropyl (4-hydroxy-2-(pyridazin-3-yl)pyrimidine-5-carboxamido)(phenyl)methyl phosphonate

Base Information

Chemical Name:diisopropyl (4-hydroxy-2-(pyridazin-3-yl)pyrimidine-5-carboxamido)(phenyl)methyl phosphonate
CAS No.:1428527-52-9
Molecular Formula:C₂₂H₂₆N₅O₅P
Molecular Weight:471.453
Hs Code.:

Synonyms:diisopropyl (4-hydroxy-2-(pyridazin-3-yl)pyrimidine-5-carboxamido)(phenyl)methyl phosphonate

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Chemical Property of diisopropyl (4-hydroxy-2-(pyridazin-3-yl)pyrimidine-5-carboxamido)(phenyl)methyl phosphonate

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Technology Process of diisopropyl (4-hydroxy-2-(pyridazin-3-yl)pyrimidine-5-carboxamido)(phenyl)methyl phosphonate

There total 8 articles about diisopropyl (4-hydroxy-2-(pyridazin-3-yl)pyrimidine-5-carboxamido)(phenyl)methyl phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 1187992-93-3
4-hydroxy-2-(pyridazin-3-yl)pyrimidine-5-carboxylic acid

: 112564-57-5
diisopropyl [amino(phenyl)methyl]phosphonate

: 1428527-52-9
diisopropyl (4-hydroxy-2-(pyridazin-3-yl)pyrimidine-5-carboxamido)(phenyl)methyl phosphonate

Guidance literature:: 4-hydroxy-2-(pyridazin-3-yl)pyrimidine-5-carboxylic acid; With thionyl chloride; at 65 ℃; for 4h;

diisopropyl [amino(phenyl)methyl]phosphonate; With triethylamine; In dichloromethane; at 25 ℃;

Reference yield:

: 1345019-59-1
C₉H₅ClN₄O₂

: 112564-57-5
diisopropyl [amino(phenyl)methyl]phosphonate

: 1428527-52-9
diisopropyl (4-hydroxy-2-(pyridazin-3-yl)pyrimidine-5-carboxamido)(phenyl)methyl phosphonate

Guidance literature:: With triethylamine; In dichloromethane; at 25 ℃;

Reference yield:

: 100-52-7
benzaldehyde

: 1428527-52-9
diisopropyl (4-hydroxy-2-(pyridazin-3-yl)pyrimidine-5-carboxamido)(phenyl)methyl phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium acetate / ethanol / 48 h / 20 - 60 °C / Molecular sieve

2: triethylamine / dichloromethane / 25 °C

With ammonium acetate; triethylamine; In ethanol; dichloromethane;