1-(4-methoxybenzyl)indolin-5-yl 4-isopropylphenylcarbamate

Base Information

Chemical Name:1-(4-methoxybenzyl)indolin-5-yl 4-isopropylphenylcarbamate
CAS No.:1239323-28-4
Molecular Formula:C₂₆H₂₈N₂O₃
Molecular Weight:416.52
Hs Code.:

Synonyms:1-(4-methoxybenzyl)indolin-5-yl 4-isopropylphenylcarbamate

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Chemical Property of 1-(4-methoxybenzyl)indolin-5-yl 4-isopropylphenylcarbamate

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Technology Process of 1-(4-methoxybenzyl)indolin-5-yl 4-isopropylphenylcarbamate

There total 3 articles about 1-(4-methoxybenzyl)indolin-5-yl 4-isopropylphenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1239323-27-3
indolin-5-yl 4-isopropylphenylcarbamate

: 123-11-5
4-methoxy-benzaldehyde

: 1239323-28-4
1-(4-methoxybenzyl)indolin-5-yl 4-isopropylphenylcarbamate

Guidance literature:: indolin-5-yl 4-isopropylphenylcarbamate; 4-methoxy-benzaldehyde; In dichloromethane; at 20 ℃; for 0.0333333h;

With sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane; for 0.5h;

Reference yield:

: 161460-40-8
1-benzylindolin-5-ol

: 1239323-28-4
1-(4-methoxybenzyl)indolin-5-yl 4-isopropylphenylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium / diethyl ether / 0.03 h / 20 °C

2.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / isopropyl alcohol; water / 20 °C / 760.05 Torr / Inert atmosphere

3.1: dichloromethane / 0.03 h / 20 °C

3.2: 0.5 h

With hydrogenchloride; hydrogen; sodium; palladium 10% on activated carbon; In diethyl ether; dichloromethane; water; isopropyl alcohol;

Reference yield:

: 74492-44-7
1-benzyl-5-methoxyindoline

: 1239323-28-4
1-(4-methoxybenzyl)indolin-5-yl 4-isopropylphenylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen bromide; acetic acid / 22 h / 20 - 115 °C

2.1: sodium / diethyl ether / 0.03 h / 20 °C

3.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / isopropyl alcohol; water / 20 °C / 760.05 Torr / Inert atmosphere

4.1: dichloromethane / 0.03 h / 20 °C

4.2: 0.5 h

With hydrogenchloride; hydrogen bromide; hydrogen; sodium; acetic acid; palladium 10% on activated carbon; In diethyl ether; dichloromethane; water; isopropyl alcohol;