N-tert-butoxycarbonyl-L-phenylalanine-L-aspartate dibenzyllester

Base Information

Chemical Name:N-tert-butoxycarbonyl-L-phenylalanine-L-aspartate dibenzyllester
CAS No.:145435-30-9
Molecular Formula:C₃₂H₃₆N₂O₇
Molecular Weight:560.647
Hs Code.:

Synonyms:N-tert-butoxycarbonyl-L-phenylalanine-L-aspartate dibenzyllester

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Chemical Property of N-tert-butoxycarbonyl-L-phenylalanine-L-aspartate dibenzyllester

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Technology Process of N-tert-butoxycarbonyl-L-phenylalanine-L-aspartate dibenzyllester

There total 4 articles about N-tert-butoxycarbonyl-L-phenylalanine-L-aspartate dibenzyllester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 2886-33-1
dibenzyl L-aspartate toluene-4-sulphonate

: 145435-30-9
N-tert-butoxycarbonyl-L-phenylalanine-L-aspartate dibenzyllester

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.ejmech.2008.01.032

Reference yield: 57.0%

: (4-hydroxyphenyl)(methyl)(benzyl)sulfonium chloride

: Boc-Phe-Asp-OH

: 145435-30-9
N-tert-butoxycarbonyl-L-phenylalanine-L-aspartate dibenzyllester

Guidance literature:: With potassium carbonate; In dichloromethane; for 8h; Ambient temperature;
DOI:10.1246/bcsj.69.1099

Reference yield:

: 637-89-8
4-sulfanylphenol

: 145435-30-9
N-tert-butoxycarbonyl-L-phenylalanine-L-aspartate dibenzyllester

Guidance literature:: Multi-step reaction with 3 steps

1: NaOH

2: 85 percent / methanol / 72 h / 35 °C

3: 57 percent / K₂CO₃ / CH₂Cl₂ / 8 h / Ambient temperature

With sodium hydroxide; potassium carbonate; In methanol; dichloromethane;
DOI:10.1246/bcsj.69.1099