[(2,6-diisopropylphenylimido)MoH(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)]

Base Information

Chemical Name:[(2,6-diisopropylphenylimido)MoH(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)]
CAS No.:1297529-16-8
Molecular Formula:C₃₅H₅₃MoN₂PSi
Molecular Weight:656.818
Hs Code.:

Synonyms:[(2,6-diisopropylphenylimido)MoH(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)]

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Chemical Property of [(2,6-diisopropylphenylimido)MoH(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)]

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Technology Process of [(2,6-diisopropylphenylimido)MoH(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)]

There total 4 articles about [(2,6-diisopropylphenylimido)MoH(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1088439-24-0
[(2,6-diisopropylphenylimido)Mo(ethyl)(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)]

: 694-53-1
phenylsilane

: 1297529-16-8
[(2,6-diisopropylphenylimido)MoH(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)]

Guidance literature:: With P(CH₃)3; In toluene; byproducts: C6H5SiH2CH2CH3, (C6H5)2SiH2, SiH4; (inert atm.); addn. of phenylsilane and trimethylphosphine to toluene soln. of molybdenum compd., heating at 50°C overnight; evapn., extn. (hexanes), evapn., NMR;
DOI:10.1021/ja111005r

Reference yield:

: 1088439-24-0
[(2,6-diisopropylphenylimido)Mo(ethyl)(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)]

: 766-08-5,146088-00-8
methylphenylsilane

: 1297529-16-8
[(2,6-diisopropylphenylimido)MoH(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)]

Guidance literature:: With P(CH₃)3; In benzene-d6; byproducts: C6H5SiH(CH3)CH2CH3; (inert atm.); addn. of methylphenylsilane and trimethylphosphine to C6D6soln. of molybdenum compd., heating at 50°C overnight; NMR;
DOI:10.1021/ja111005r

Reference yield:

: 1088439-24-0
[(2,6-diisopropylphenylimido)Mo(ethyl)(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)]

: 1297529-16-8
[(2,6-diisopropylphenylimido)MoH(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)]

Guidance literature:: In benzene-d6; byproducts: CH2CH2; (inert atm.); heating C6D6 soln. of molybdenum compd. at 50°C overnight; NMR;
DOI:10.1021/ja111005r