[(2,6-diisopropylphenylimido)Mo(ethyl)(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)]

Base Information

Chemical Name:[(2,6-diisopropylphenylimido)Mo(ethyl)(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)]
CAS No.:1088439-24-0
Molecular Formula:C₃₇H₅₇MoN₂PSi
Molecular Weight:684.872
Hs Code.:

Synonyms:[(2,6-diisopropylphenylimido)Mo(ethyl)(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)]

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Chemical Property of [(2,6-diisopropylphenylimido)Mo(ethyl)(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)]

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Technology Process of [(2,6-diisopropylphenylimido)Mo(ethyl)(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)]

There total 3 articles about [(2,6-diisopropylphenylimido)Mo(ethyl)(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 74-85-1
ethene

: 1297529-06-6,1088439-22-8
[(2,6-diisopropylphenylimido)Mo(phenylsilanide)(PMe3)(η3-N(2,6-diisopropylphenyl)SiH2Ph)]

: 1088439-24-0
[(2,6-diisopropylphenylimido)Mo(ethyl)(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)]

Guidance literature:: In diethyl ether; byproducts: C6H5SiH3; (inert atm.); addn. of ethylene to ethereal soln. of molybdenum compd. at -80°C, stirring at room temp. for 12 h; evapn., drying, extn. (hexane), concg., keeping at -30°C overnight, filtration, washing with cold hexanes, drying in vac., elem. anal.;
DOI:10.1021/ja111005r

Reference yield: 48.0%

: [(2,6-diisopropylphenylimido)2Mo(PMe3)2(η2-ethylene)]

: 74-85-1
ethene

: 694-53-1
phenylsilane

: 1088439-24-0
[(2,6-diisopropylphenylimido)Mo(ethyl)(PMe3)(η3-N(2,6-diisopropylphenyl)SiH(Ph)CHCH2)]

Guidance literature:: In diethyl ether; byproducts: P(CH3)3, H2; (inert atm.); addn. of phenylsilane to ethereal soln. of molybdenum compd. at -80°C, freezing at -196°C, addn. of ethylene, stirring at room temp. for 3 d; evapn., extn. (hexane), concg., keeping at -30°C for 2 d, filtration, drying in vac., elem. anal.;
DOI:10.1021/ja111005r