1-(3-azido-2,3-dideoxy-5-O-p-monomethoxy-trityl-β-D-erythro-pentofuranosyl)-6,7-diphenyllumazine

Base Information

Chemical Name:1-(3-azido-2,3-dideoxy-5-O-p-monomethoxy-trityl-β-D-erythro-pentofuranosyl)-6,7-diphenyllumazine
CAS No.:159227-97-1
Molecular Formula:C₄₃H₃₅N₇O₅
Molecular Weight:729.795
Hs Code.:

Synonyms:1-(3-azido-2,3-dideoxy-5-O-p-monomethoxy-trityl-β-D-erythro-pentofuranosyl)-6,7-diphenyllumazine

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Chemical Property of 1-(3-azido-2,3-dideoxy-5-O-p-monomethoxy-trityl-β-D-erythro-pentofuranosyl)-6,7-diphenyllumazine

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Technology Process of 1-(3-azido-2,3-dideoxy-5-O-p-monomethoxy-trityl-β-D-erythro-pentofuranosyl)-6,7-diphenyllumazine

There total 13 articles about 1-(3-azido-2,3-dideoxy-5-O-p-monomethoxy-trityl-β-D-erythro-pentofuranosyl)-6,7-diphenyllumazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 159227-96-0
1-(2-deoxy-3-O-mesyl-5-O-p-monomethoxytrityl-β-D-threo-pentofuranosyl)-6,7-diphenyllumazine

: 159227-97-1
1-(3-azido-2,3-dideoxy-5-O-p-monomethoxy-trityl-β-D-erythro-pentofuranosyl)-6,7-diphenyllumazine

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 80 ℃;
DOI:10.1080/15257779408013278

Reference yield:

: 50255-88-4
6,7-diphenyl-2,4-bis-trimethylsilanyloxy-pteridine

: 159227-97-1
1-(3-azido-2,3-dideoxy-5-O-p-monomethoxy-trityl-β-D-erythro-pentofuranosyl)-6,7-diphenyllumazine

Guidance literature:: Multi-step reaction with 8 steps

1: BF₃*OEt₂ / ethyl acetate / 2 h / Ambient temperature

2: 72 percent / pyridine, acetic acid, hydrazine monohydrate / 22 h / Ambient temperature

3: 92 percent / DMAP / acetonitrile / 0.17 h

4: 73 percent / AIBN, n-Bu₃SnH / toluene / 1.5 h / Heating

5: 84 percent / sodium methoxide

6: 69 percent / pyridine

7: 84 percent / pyridine / 2 h / Ambient temperature

8: 70 percent / sodium azide / dimethylformamide / 80 °C

With pyridine; dmap; sodium azide; 2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; tri-n-butyl-tin hydride; sodium methylate; hydrazine hydrate; acetic acid; In pyridine; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1080/15257779408013278

Reference yield:

: 14892-98-9
6,7-diphenylpteridine-2,4(1H,3H)-dione

: 159227-97-1
1-(3-azido-2,3-dideoxy-5-O-p-monomethoxy-trityl-β-D-erythro-pentofuranosyl)-6,7-diphenyllumazine

Guidance literature:: Multi-step reaction with 9 steps

1: ammonium sulfate / Heating

2: BF₃*OEt₂ / ethyl acetate / 2 h / Ambient temperature

3: 72 percent / pyridine, acetic acid, hydrazine monohydrate / 22 h / Ambient temperature

4: 92 percent / DMAP / acetonitrile / 0.17 h

5: 73 percent / AIBN, n-Bu₃SnH / toluene / 1.5 h / Heating

6: 84 percent / sodium methoxide

7: 69 percent / pyridine

8: 84 percent / pyridine / 2 h / Ambient temperature

9: 70 percent / sodium azide / dimethylformamide / 80 °C

With pyridine; dmap; ammonium sulfate; sodium azide; 2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; tri-n-butyl-tin hydride; sodium methylate; hydrazine hydrate; acetic acid; In pyridine; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1080/15257779408013278