4-fluorobenzoic acid iodomethyl ester

Base Information

Chemical Name:4-fluorobenzoic acid iodomethyl ester
CAS No.:1239712-04-9
Molecular Formula:C₈H₆FIO₂
Molecular Weight:280.037
Hs Code.:

Synonyms:4-fluorobenzoic acid iodomethyl ester

Suppliers and Price of 4-fluorobenzoic acid iodomethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-fluorobenzoic acid iodomethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-fluorobenzoic acid iodomethyl ester

There total 2 articles about 4-fluorobenzoic acid iodomethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: chloromethyl 4-fluorobenzoate

: 1239712-04-9
4-fluorobenzoic acid iodomethyl ester

Guidance literature:: With sodium iodide; In acetone;

Reference yield: 33.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 403-43-0
4-fluorobenzoyl chloride

: 1239712-04-9
4-fluorobenzoic acid iodomethyl ester

Guidance literature:: formaldehyd; 4-fluorobenzoyl chloride; With zinc(II) chloride; at 55 ℃; for 24h; Inert atmosphere;

With sodium iodide; In acetone; at 20 ℃; for 4.5h; Inert atmosphere; Darkness;
DOI:10.1021/ol101519w

Reference yield: 72.0%

: 1239712-04-9
4-fluorobenzoic acid iodomethyl ester

: 623-91-6
diethyl Fumarate

: 4-(4-fluorobenzoyl)-5-oxo-tetrahydro-furan-3-carboxylic acid ethyl ester

Guidance literature:: 4-fluorobenzoic acid iodomethyl ester; diethyl Fumarate; With dimethyl zinc(II); oxygen; In n-heptane; dichloromethane; at 20 ℃; for 20h;

With water; ammonium chloride; In n-heptane; dichloromethane; stereoselective reaction;
DOI:10.1021/ol101519w