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(C5H5)((CH3)2CH)CH2((C6H5)3P)(NO)Re

Base Information Edit
  • Chemical Name:(C5H5)((CH3)2CH)CH2((C6H5)3P)(NO)Re
  • CAS No.:85926-74-5
  • Molecular Formula:C27H29NOPRe
  • Molecular Weight:600.714
  • Hs Code.:
  • Mol file:85926-74-5.mol
(C<sub>5</sub>H<sub>5</sub>)((CH<sub>3</sub>)2CH)CH<sub>2</sub>((C<sub>6</sub>H<sub>5</sub>)3P)(NO)Re

Synonyms:(C5H5)((CH3)2CH)CH2((C6H5)3P)(NO)Re

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Chemical Property of (C5H5)((CH3)2CH)CH2((C6H5)3P)(NO)Re Edit
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Technology Process of (C5H5)((CH3)2CH)CH2((C6H5)3P)(NO)Re

There total 4 articles about (C5H5)((CH3)2CH)CH2((C6H5)3P)(NO)Re which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In tetrahydrofuran; addn. of 2 equiv. LiCuMe2 to Re-complex (-80°C, stirring), removal of cooling bath (after 0. 5 h), standing for 12 h; solvent removal (reduced pressure), benzene addn., filtration (Celite),solvent removal from filtrate (reduced pressure), chromy. (SiO2, AcOEt/hexane=5/95 v/v), solvent removal (reduced pressure);
DOI:10.1039/DT9950001857
Guidance literature:
In dichloromethane; pentane; to CH2Cl2 at -78°C was added Re-complex, (CH3)2CHLi was added, stirred for 30 min at -78°C, warmed to room temp.; evapd., extd. with C6H6, filtered through silica gel, evapd., chromd. (silica gel, CH2Cl2/hexanes);
DOI:10.1021/ja00353a020
Guidance literature:
In dichloromethane; pentane; to CH2Cl2 at -78°C was added Re-complex, (CH3)3CLi was added, stirred for 30 min at -78°C, warmed to room temp.; evapd., extd. with C6H6, filtered through silica gel, evapd., chromd. (silica gel, CH2Cl2/hexanes);
DOI:10.1021/ja00353a020
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