1-(naphthyl-2-yl)ethylidene-2-[4-(5-methyl-1-p-tolyl-1,2,3-triazol-4-yl)thiazol-2-yl]hydraziane

Base Information

Chemical Name:1-(naphthyl-2-yl)ethylidene-2-[4-(5-methyl-1-p-tolyl-1,2,3-triazol-4-yl)thiazol-2-yl]hydraziane
CAS No.:1516632-35-1
Molecular Formula:C₂₅H₂₂N₆S
Molecular Weight:438.556
Hs Code.:

Synonyms:1-(naphthyl-2-yl)ethylidene-2-[4-(5-methyl-1-p-tolyl-1,2,3-triazol-4-yl)thiazol-2-yl]hydraziane

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Chemical Property of 1-(naphthyl-2-yl)ethylidene-2-[4-(5-methyl-1-p-tolyl-1,2,3-triazol-4-yl)thiazol-2-yl]hydraziane

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Technology Process of 1-(naphthyl-2-yl)ethylidene-2-[4-(5-methyl-1-p-tolyl-1,2,3-triazol-4-yl)thiazol-2-yl]hydraziane

There total 4 articles about 1-(naphthyl-2-yl)ethylidene-2-[4-(5-methyl-1-p-tolyl-1,2,3-triazol-4-yl)thiazol-2-yl]hydraziane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1109276-86-9
2-bromo-1-(5-methyl-1-(p-tolyl)-1H-1,2,3-triazole-4-yl)ethan-1-one

: 133477-39-1
2-[1-(2-naphthenyl)ethyledene]hydrazinecarbothioamide

: 1516632-35-1
1-(naphthyl-2-yl)ethylidene-2-[4-(5-methyl-1-p-tolyl-1,2,3-triazol-4-yl)thiazol-2-yl]hydraziane

Guidance literature:: In ethanol; at 60 ℃; for 0.166667h; Reflux;
DOI:10.2174/157017861010131126115715

Reference yield:

: 2101-86-2
p-methylazidobenzene

: 1516632-35-1
1-(naphthyl-2-yl)ethylidene-2-[4-(5-methyl-1-p-tolyl-1,2,3-triazol-4-yl)thiazol-2-yl]hydraziane

Guidance literature:: Multi-step reaction with 3 steps

1: sodium ethanolate / 1 h / 0 °C

2: hydrogenchloride; bromine / water; chloroform / Cooling

3: ethanol / 0.17 h / 60 °C / Reflux

With hydrogenchloride; bromine; sodium ethanolate; In ethanol; chloroform; water;
DOI:10.2174/157017861010131126115715

Reference yield:

: 1-[5-methyl-1-(p-tolyl)-1H-1,2,3-triazol-4-yl]ethanone

: 1516632-35-1
1-(naphthyl-2-yl)ethylidene-2-[4-(5-methyl-1-p-tolyl-1,2,3-triazol-4-yl)thiazol-2-yl]hydraziane

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; bromine / water; chloroform / Cooling

2: ethanol / 0.17 h / 60 °C / Reflux

With hydrogenchloride; bromine; In ethanol; chloroform; water;
DOI:10.2174/157017861010131126115715