2,2-dimethylpropionic acid 4-({[5-[2-(6-tert-butoxycarbonylmethyl-2,2-dimethyl-[1,3]dioxan-4-yl)vinyl]-4-(4-fluorophenyl)-1-isopropyl-3-phenyl-1H-pyrrole-2-carbonyl]amino}methyl)benzyl ester

Base Information

Chemical Name:2,2-dimethylpropionic acid 4-({[5-[2-(6-tert-butoxycarbonylmethyl-2,2-dimethyl-[1,3]dioxan-4-yl)vinyl]-4-(4-fluorophenyl)-1-isopropyl-3-phenyl-1H-pyrrole-2-carbonyl]amino}methyl)benzyl ester
CAS No.:855249-15-9
Molecular Formula:C₄₇H₅₇FN₂O₇
Molecular Weight:780.977
Hs Code.:

2,2-dimethylpropionic acid 4-({[5-[2-(6-tert-butoxycarbonylmethyl-2,2-dimethyl-[1,3]dioxan-4-yl)vinyl]-4-(4-fluorophenyl)-1-isopropyl-3-phenyl-1H-pyrrole-2-carbonyl]amino}methyl)benzyl ester

Synonyms:2,2-dimethylpropionic acid 4-({[5-[2-(6-tert-butoxycarbonylmethyl-2,2-dimethyl-[1,3]dioxan-4-yl)vinyl]-4-(4-fluorophenyl)-1-isopropyl-3-phenyl-1H-pyrrole-2-carbonyl]amino}methyl)benzyl ester

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Chemical Property of 2,2-dimethylpropionic acid 4-({[5-[2-(6-tert-butoxycarbonylmethyl-2,2-dimethyl-[1,3]dioxan-4-yl)vinyl]-4-(4-fluorophenyl)-1-isopropyl-3-phenyl-1H-pyrrole-2-carbonyl]amino}methyl)benzyl ester

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Technology Process of 2,2-dimethylpropionic acid 4-({[5-[2-(6-tert-butoxycarbonylmethyl-2,2-dimethyl-[1,3]dioxan-4-yl)vinyl]-4-(4-fluorophenyl)-1-isopropyl-3-phenyl-1H-pyrrole-2-carbonyl]amino}methyl)benzyl ester

There total 1 articles about 2,2-dimethylpropionic acid 4-({[5-[2-(6-tert-butoxycarbonylmethyl-2,2-dimethyl-[1,3]dioxan-4-yl)vinyl]-4-(4-fluorophenyl)-1-isopropyl-3-phenyl-1H-pyrrole-2-carbonyl]amino}methyl)benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 855249-14-8
[5-[4-(2,2-dimethylpropionyloxymethyl)benzylcarbamoyl]-3-(4-fluorophenyl)-1-isopropyl-4-phenyl-1H-pyrrol-2-ylmethyl]triphenylphosphonium bromide

: 124752-23-4
tert-butyl 2-[(4R,6S)-6-formyl-2,2-dimethyl-1,3-dioxan-4-yl]acetate

: 855249-15-9
2,2-dimethylpropionic acid 4-({[5-[2-(6-tert-butoxycarbonylmethyl-2,2-dimethyl-[1,3]dioxan-4-yl)vinyl]-4-(4-fluorophenyl)-1-isopropyl-3-phenyl-1H-pyrrole-2-carbonyl]amino}methyl)benzyl ester

Guidance literature:: [5-[4-(2,2-dimethylpropionyloxymethyl)benzylcarbamoyl]-3-(4-fluorophenyl)-1-isopropyl-4-phenyl-1H-pyrrol-2-ylmethyl]triphenylphosphonium bromide; With sodium hexamethyldisilazane; In tetrahydrofuran; dimethyl sulfoxide; at -78 ℃; for 0.0833333h;

tert-butyl 2-[(4R,6S)-6-formyl-2,2-dimethyl-1,3-dioxan-4-yl]acetate; In tetrahydrofuran; dimethyl sulfoxide; at -78 - 25 ℃; for 2h;

With ammonium chloride; In tetrahydrofuran; water; dimethyl sulfoxide;

Reference yield: 72.0%

: 855249-15-9
2,2-dimethylpropionic acid 4-({[5-[2-(6-tert-butoxycarbonylmethyl-2,2-dimethyl-[1,3]dioxan-4-yl)vinyl]-4-(4-fluorophenyl)-1-isopropyl-3-phenyl-1H-pyrrole-2-carbonyl]amino}methyl)benzyl ester

: 855249-16-0
(6-{2-[3-(4-fluorophenyl)-5-(4-hydroxymethylbenzylcarbamoyl)-1-isopropyl-4-phenyl-1H-pyrrol-2-yl]vinyl}-2,2-dimethyl-[1,3]dioxan-4-yl)acetic acid tert-butyl ester

Guidance literature:: 2,2-dimethylpropionic acid 4-({[5-[2-(6-tert-butoxycarbonylmethyl-2,2-dimethyl-[1,3]dioxan-4-yl)vinyl]-4-(4-fluorophenyl)-1-isopropyl-3-phenyl-1H-pyrrole-2-carbonyl]amino}methyl)benzyl ester; With methanol; sodium hydroxide; water; at 20 ℃; for 24h;

With sodium hydrogencarbonate; In dichloromethane; water;