(RS)-1,3-Bis-(4-nitrobenzyl)-5-(3-brom-2-oxo-propyl)-5-(1-methylbutyl)-2,4,6(1H,3H,5H)-pyrimidintrion

Base Information

Chemical Name:(RS)-1,3-Bis-(4-nitrobenzyl)-5-(3-brom-2-oxo-propyl)-5-(1-methylbutyl)-2,4,6(1H,3H,5H)-pyrimidintrion
CAS No.:143389-39-3
Molecular Formula:C₂₆H₂₇BrN₄O₈
Molecular Weight:603.426
Hs Code.:

Synonyms:(RS)-1,3-Bis-(4-nitrobenzyl)-5-(3-brom-2-oxo-propyl)-5-(1-methylbutyl)-2,4,6(1H,3H,5H)-pyrimidintrion

Suppliers and Price of (RS)-1,3-Bis-(4-nitrobenzyl)-5-(3-brom-2-oxo-propyl)-5-(1-methylbutyl)-2,4,6(1H,3H,5H)-pyrimidintrion

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (RS)-1,3-Bis-(4-nitrobenzyl)-5-(3-brom-2-oxo-propyl)-5-(1-methylbutyl)-2,4,6(1H,3H,5H)-pyrimidintrion

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (RS)-1,3-Bis-(4-nitrobenzyl)-5-(3-brom-2-oxo-propyl)-5-(1-methylbutyl)-2,4,6(1H,3H,5H)-pyrimidintrion

There total 4 articles about (RS)-1,3-Bis-(4-nitrobenzyl)-5-(3-brom-2-oxo-propyl)-5-(1-methylbutyl)-2,4,6(1H,3H,5H)-pyrimidintrion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 143389-28-0,143389-35-9
(1'RS,2SR und 1'RS,2RS)-1,3-Bis-(4-nitrobenzyl)-5-(3-brom-2-hydroxy-propyl)-5-(1-methylbutyl)-2,4,6(1H,3H,5H)-pyrimidintrion

: 143389-39-3
(RS)-1,3-Bis-(4-nitrobenzyl)-5-(3-brom-2-oxo-propyl)-5-(1-methylbutyl)-2,4,6(1H,3H,5H)-pyrimidintrion

Guidance literature:: With chromium(VI) oxide; In acetic acid; for 0.333333h; Heating;
DOI:10.1002/ardp.19923250508

Reference yield:

: 143389-33-7
(RS)-1,3-Bis-(4-nitrobenzyl)-5-(1-methylbutyl)-5-(2-propenyl)-2,4,6(1H,3H,5H)-pyrimidintrion

: 143389-39-3
(RS)-1,3-Bis-(4-nitrobenzyl)-5-(3-brom-2-oxo-propyl)-5-(1-methylbutyl)-2,4,6(1H,3H,5H)-pyrimidintrion

Guidance literature:: Multi-step reaction with 2 steps

1: 10 percent / 0.1 N KBr/KBrO₃ soln., concd. HCl / CHCl₃ / 2 h

2: 58 percent / CrO₃ / acetic acid / 0.33 h / Heating

With potassium bromate; chromium(VI) oxide; hydrogenchloride; potassium bromide; In chloroform; acetic acid;
DOI:10.1002/ardp.19923250508

Reference yield:

: 100-14-1
4-nitrobenzyl chloride

: 143389-39-3
(RS)-1,3-Bis-(4-nitrobenzyl)-5-(3-brom-2-oxo-propyl)-5-(1-methylbutyl)-2,4,6(1H,3H,5H)-pyrimidintrion

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / 10percent aq. Na₂CO₃ / ethanol / 0.5 h / Heating

2: 10 percent / 0.1 N KBr/KBrO₃ soln., concd. HCl / CHCl₃ / 2 h

3: 58 percent / CrO₃ / acetic acid / 0.33 h / Heating

With potassium bromate; chromium(VI) oxide; hydrogenchloride; sodium carbonate; potassium bromide; In ethanol; chloroform; acetic acid;
DOI:10.1002/ardp.19923250508