(1'RS,2SR und 1'RS,2RS)-1,3-Bis-(4-nitrobenzyl)-5-(3-brom-2-hydroxy-propyl)-5-(1-methylbutyl)-2,4,6(1H,3H,5H)-pyrimidintrion

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Chemical Name:(1'RS,2SR und 1'RS,2RS)-1,3-Bis-(4-nitrobenzyl)-5-(3-brom-2-hydroxy-propyl)-5-(1-methylbutyl)-2,4,6(1H,3H,5H)-pyrimidintrion
CAS No.:143389-28-0
Molecular Formula:C₂₆H₂₉BrN₄O₈
Molecular Weight:605.442
Hs Code.:

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Chemical Property of (1'RS,2SR und 1'RS,2RS)-1,3-Bis-(4-nitrobenzyl)-5-(3-brom-2-hydroxy-propyl)-5-(1-methylbutyl)-2,4,6(1H,3H,5H)-pyrimidintrion

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Technology Process of (1'RS,2SR und 1'RS,2RS)-1,3-Bis-(4-nitrobenzyl)-5-(3-brom-2-hydroxy-propyl)-5-(1-methylbutyl)-2,4,6(1H,3H,5H)-pyrimidintrion

There total 3 articles about (1'RS,2SR und 1'RS,2RS)-1,3-Bis-(4-nitrobenzyl)-5-(3-brom-2-hydroxy-propyl)-5-(1-methylbutyl)-2,4,6(1H,3H,5H)-pyrimidintrion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 143389-33-7
(RS)-1,3-Bis-(4-nitrobenzyl)-5-(1-methylbutyl)-5-(2-propenyl)-2,4,6(1H,3H,5H)-pyrimidintrion

: 143389-28-0,143389-35-9
(1'RS,2SR und 1'RS,2RS)-1,3-Bis-(4-nitrobenzyl)-5-(3-brom-2-hydroxy-propyl)-5-(1-methylbutyl)-2,4,6(1H,3H,5H)-pyrimidintrion

Guidance literature:: With potassium bromate; hydrogenchloride; potassium bromide; In chloroform; for 2h;
DOI:10.1002/ardp.19923250508

Reference yield:

: 100-14-1
4-nitrobenzyl chloride

: 143389-28-0,143389-35-9
(1'RS,2SR und 1'RS,2RS)-1,3-Bis-(4-nitrobenzyl)-5-(3-brom-2-hydroxy-propyl)-5-(1-methylbutyl)-2,4,6(1H,3H,5H)-pyrimidintrion

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / 10percent aq. Na₂CO₃ / ethanol / 0.5 h / Heating

2: 10 percent / 0.1 N KBr/KBrO₃ soln., concd. HCl / CHCl₃ / 2 h

With potassium bromate; hydrogenchloride; sodium carbonate; potassium bromide; In ethanol; chloroform;
DOI:10.1002/ardp.19923250508

Reference yield:

: 309-43-3,51165-35-6,51165-36-7,51165-37-8,64915-87-3
Sodium secobarbital

: 143389-28-0,143389-35-9
(1'RS,2SR und 1'RS,2RS)-1,3-Bis-(4-nitrobenzyl)-5-(3-brom-2-hydroxy-propyl)-5-(1-methylbutyl)-2,4,6(1H,3H,5H)-pyrimidintrion

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / 10percent aq. Na₂CO₃ / ethanol / 0.5 h / Heating

2: 10 percent / 0.1 N KBr/KBrO₃ soln., concd. HCl / CHCl₃ / 2 h

With potassium bromate; hydrogenchloride; sodium carbonate; potassium bromide; In ethanol; chloroform;
DOI:10.1002/ardp.19923250508