11-(Phenylsulfonyl)-6,11-dihydro-5H-pyrido[3',2':4,5]pyrrolo[3,2-c]quinolin-6-one

Base Information

Chemical Name:11-(Phenylsulfonyl)-6,11-dihydro-5H-pyrido[3',2':4,5]pyrrolo[3,2-c]quinolin-6-one
CAS No.:278593-23-0
Molecular Formula:C₂₀H₁₃N₃O₃S
Molecular Weight:375.408
Hs Code.:

Synonyms:11-(Phenylsulfonyl)-6,11-dihydro-5H-pyrido[3',2':4,5]pyrrolo[3,2-c]quinolin-6-one

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Chemical Property of 11-(Phenylsulfonyl)-6,11-dihydro-5H-pyrido[3',2':4,5]pyrrolo[3,2-c]quinolin-6-one

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Technology Process of 11-(Phenylsulfonyl)-6,11-dihydro-5H-pyrido[3',2':4,5]pyrrolo[3,2-c]quinolin-6-one

There total 4 articles about 11-(Phenylsulfonyl)-6,11-dihydro-5H-pyrido[3',2':4,5]pyrrolo[3,2-c]quinolin-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 278593-21-8
tert-Butyl N-(2-iodophenyl)-N-{[1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-3-yl]carbonyl}carbamate

: 278593-23-0
11-(Phenylsulfonyl)-6,11-dihydro-5H-pyrido[3',2':4,5]pyrrolo[3,2-c]quinolin-6-one

Guidance literature:: With triphenylphosphine; silver carbonate; palladium diacetate; In N,N-dimethyl-formamide; at 100 ℃; for 24h;
DOI:10.1055/s-2000-6374

Reference yield:

: 155819-08-2
1-(benzenesulfonyl)-1H-pyrrolo[2,3-b]pyridine-3-carboxaldehyde

: 278593-23-0
11-(Phenylsulfonyl)-6,11-dihydro-5H-pyrido[3',2':4,5]pyrrolo[3,2-c]quinolin-6-one

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / NaClO₂; H₂O; sulfamic acid / dioxane / 20 °C

2: 79 percent / DMAP; EDCI*HCl / CH₂Cl₂ / 20 °C

3: 97 percent / DMAP; Et₃N / acetonitrile / 16 h / 20 °C

4: 72 percent / triphenylphosphine; Ag₂CO₃ / Pd(OAc)2 / dimethylformamide / 24 h / 100 °C

With dmap; sodium chlorite; aminosulfonic acid; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; silver carbonate; palladium diacetate; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 1: Oxidation / 2: Acylation / 3: Acylation / 4: Cyclization;
DOI:10.1055/s-2000-6374

Reference yield:

: 245064-80-6
1-Phenylsulfonylpyrrolo[2,3-b]pyridine-3-carboxylic acid

: 278593-23-0
11-(Phenylsulfonyl)-6,11-dihydro-5H-pyrido[3',2':4,5]pyrrolo[3,2-c]quinolin-6-one

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / DMAP; EDCI*HCl / CH₂Cl₂ / 20 °C

2: 97 percent / DMAP; Et₃N / acetonitrile / 16 h / 20 °C

3: 72 percent / triphenylphosphine; Ag₂CO₃ / Pd(OAc)2 / dimethylformamide / 24 h / 100 °C

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; silver carbonate; palladium diacetate; In dichloromethane; N,N-dimethyl-formamide; acetonitrile; 1: Acylation / 2: Acylation / 3: Cyclization;
DOI:10.1055/s-2000-6374