11-(Phenylsulfonyl)-11H-pyrido[3',2':4,5]pyrrolo[3,2-c]quinolin-6-yl trifluoromethanesulfonate

Base Information

Chemical Name:11-(Phenylsulfonyl)-11H-pyrido[3',2':4,5]pyrrolo[3,2-c]quinolin-6-yl trifluoromethanesulfonate
CAS No.:278593-26-3
Molecular Formula:C₂₁H₁₂F₃N₃O₅S₂
Molecular Weight:507.471
Hs Code.:

Synonyms:11-(Phenylsulfonyl)-11H-pyrido[3',2':4,5]pyrrolo[3,2-c]quinolin-6-yl trifluoromethanesulfonate

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Chemical Property of 11-(Phenylsulfonyl)-11H-pyrido[3',2':4,5]pyrrolo[3,2-c]quinolin-6-yl trifluoromethanesulfonate

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Technology Process of 11-(Phenylsulfonyl)-11H-pyrido[3',2':4,5]pyrrolo[3,2-c]quinolin-6-yl trifluoromethanesulfonate

There total 5 articles about 11-(Phenylsulfonyl)-11H-pyrido[3',2':4,5]pyrrolo[3,2-c]quinolin-6-yl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 278593-23-0
11-(Phenylsulfonyl)-6,11-dihydro-5H-pyrido[3',2':4,5]pyrrolo[3,2-c]quinolin-6-one

: 278593-26-3
11-(Phenylsulfonyl)-11H-pyrido[3',2':4,5]pyrrolo[3,2-c]quinolin-6-yl trifluoromethanesulfonate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1055/s-2000-6374

Reference yield:

: 155819-08-2
1-(benzenesulfonyl)-1H-pyrrolo[2,3-b]pyridine-3-carboxaldehyde

: 278593-26-3
11-(Phenylsulfonyl)-11H-pyrido[3',2':4,5]pyrrolo[3,2-c]quinolin-6-yl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / NaClO₂; H₂O; sulfamic acid / dioxane / 20 °C

2: 79 percent / DMAP; EDCI*HCl / CH₂Cl₂ / 20 °C

3: 97 percent / DMAP; Et₃N / acetonitrile / 16 h / 20 °C

4: 72 percent / triphenylphosphine; Ag₂CO₃ / Pd(OAc)2 / dimethylformamide / 24 h / 100 °C

5: 79 percent / pyridine / CH₂Cl₂ / 3 h / 20 °C

With pyridine; dmap; sodium chlorite; aminosulfonic acid; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; silver carbonate; palladium diacetate; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 1: Oxidation / 2: Acylation / 3: Acylation / 4: Cyclization / 5: Substitution;
DOI:10.1055/s-2000-6374

Reference yield:

: 245064-80-6
1-Phenylsulfonylpyrrolo[2,3-b]pyridine-3-carboxylic acid

: 278593-26-3
11-(Phenylsulfonyl)-11H-pyrido[3',2':4,5]pyrrolo[3,2-c]quinolin-6-yl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: 79 percent / DMAP; EDCI*HCl / CH₂Cl₂ / 20 °C

2: 97 percent / DMAP; Et₃N / acetonitrile / 16 h / 20 °C

3: 72 percent / triphenylphosphine; Ag₂CO₃ / Pd(OAc)2 / dimethylformamide / 24 h / 100 °C

4: 79 percent / pyridine / CH₂Cl₂ / 3 h / 20 °C

With pyridine; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; silver carbonate; palladium diacetate; In dichloromethane; N,N-dimethyl-formamide; acetonitrile; 1: Acylation / 2: Acylation / 3: Cyclization / 4: Substitution;
DOI:10.1055/s-2000-6374