3-(N,N-bis(methoxycarbonylmethyl)-(2-(2-amino-5-methoxyphenoxy))-1-ethoxy)-4-(N'-methoxycarbonylmethyl)aminobenzaldehyde

Base Information

Chemical Name:3-(N,N-bis(methoxycarbonylmethyl)-(2-(2-amino-5-methoxyphenoxy))-1-ethoxy)-4-(N'-methoxycarbonylmethyl)aminobenzaldehyde
CAS No.:404335-92-8
Molecular Formula:C₂₅H₃₀N₂O₁₀
Molecular Weight:518.521
Hs Code.:

Synonyms:3-(N,N-bis(methoxycarbonylmethyl)-(2-(2-amino-5-methoxyphenoxy))-1-ethoxy)-4-(N'-methoxycarbonylmethyl)aminobenzaldehyde

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Chemical Property of 3-(N,N-bis(methoxycarbonylmethyl)-(2-(2-amino-5-methoxyphenoxy))-1-ethoxy)-4-(N'-methoxycarbonylmethyl)aminobenzaldehyde

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Technology Process of 3-(N,N-bis(methoxycarbonylmethyl)-(2-(2-amino-5-methoxyphenoxy))-1-ethoxy)-4-(N'-methoxycarbonylmethyl)aminobenzaldehyde

There total 6 articles about 3-(N,N-bis(methoxycarbonylmethyl)-(2-(2-amino-5-methoxyphenoxy))-1-ethoxy)-4-(N'-methoxycarbonylmethyl)aminobenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 96-32-2
bromoacetic acid methyl ester

: 404335-91-7
3-(2-(2-amino-5-methoxyphenoxy)-1-ethoxy)-4-aminobenzaldehyde dioxolane

: 404335-92-8
3-(N,N-bis(methoxycarbonylmethyl)-(2-(2-amino-5-methoxyphenoxy))-1-ethoxy)-4-(N'-methoxycarbonylmethyl)aminobenzaldehyde

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 90 ℃;
DOI:10.1021/ja011774y

Reference yield:

: 704-14-3
3-methoxy-6-nitro-phenol

: 404335-92-8
3-(N,N-bis(methoxycarbonylmethyl)-(2-(2-amino-5-methoxyphenoxy))-1-ethoxy)-4-(N'-methoxycarbonylmethyl)aminobenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / potassium carbonate / dimethylformamide / 3 h / 100 °C

2: 49 percent / H₂ / platinum oxide / ethyl acetate; methanol; 1,2-dichloro-ethane / 8 h / 1034.32 Torr

3: 40 percent / diisopropylethylamine / dimethylformamide / 90 °C

With hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; platinum(IV) oxide; In methanol; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/ja011774y

Reference yield:

: 704-13-2
5-formyl-2-nitrophenol

: 404335-92-8
3-(N,N-bis(methoxycarbonylmethyl)-(2-(2-amino-5-methoxyphenoxy))-1-ethoxy)-4-(N'-methoxycarbonylmethyl)aminobenzaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: 77 percent / potassium carbonate / dimethylformamide / 2 h / 100 °C

2: 97 percent / p-toluenesulfonic acid / 24 h / Heating

3: 88 percent / potassium carbonate / dimethylformamide / 3 h / 100 °C

4: 49 percent / H₂ / platinum oxide / ethyl acetate; methanol; 1,2-dichloro-ethane / 8 h / 1034.32 Torr

5: 40 percent / diisopropylethylamine / dimethylformamide / 90 °C

With hydrogen; potassium carbonate; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; platinum(IV) oxide; In methanol; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/ja011774y