Glycine, N-[2-[2-[5-(2,7-difluoro-3,6-dihydroxy-9H-xanthen-9-yl)-2-[(2-methoxy-2- oxoethyl)amino]phenoxy]ethoxy]-4-methoxyphenyl]-N-(2-methoxy-2-oxo ethyl)-, methyl ester

Base Information

Chemical Name:Glycine, N-[2-[2-[5-(2,7-difluoro-3,6-dihydroxy-9H-xanthen-9-yl)-2-[(2-methoxy-2- oxoethyl)amino]phenoxy]ethoxy]-4-methoxyphenyl]-N-(2-methoxy-2-oxo ethyl)-, methyl ester
CAS No.:404335-93-9
Molecular Formula:C37H36F2N2O12
Molecular Weight:738.696
Hs Code.:

Glycine,
N-[2-[2-[5-(2,7-difluoro-3,6-dihydroxy-9H-xanthen-9-yl)-2-[(2-methoxy-2-
oxoethyl)amino]phenoxy]ethoxy]-4-methoxyphenyl]-N-(2-methoxy-2-oxo
ethyl)-, methyl ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Glycine, N-[2-[2-[5-(2,7-difluoro-3,6-dihydroxy-9H-xanthen-9-yl)-2-[(2-methoxy-2- oxoethyl)amino]phenoxy]ethoxy]-4-methoxyphenyl]-N-(2-methoxy-2-oxo ethyl)-, methyl ester

Chemical Property:

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Safty Information:

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Technology Process of Glycine, N-[2-[2-[5-(2,7-difluoro-3,6-dihydroxy-9H-xanthen-9-yl)-2-[(2-methoxy-2- oxoethyl)amino]phenoxy]ethoxy]-4-methoxyphenyl]-N-(2-methoxy-2-oxo ethyl)-, methyl ester

There total 7 articles about Glycine, N-[2-[2-[5-(2,7-difluoro-3,6-dihydroxy-9H-xanthen-9-yl)-2-[(2-methoxy-2- oxoethyl)amino]phenoxy]ethoxy]-4-methoxyphenyl]-N-(2-methoxy-2-oxo ethyl)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 103068-41-3
4-fluororesorcinol

: 404335-92-8
3-(N,N-bis(methoxycarbonylmethyl)-(2-(2-amino-5-methoxyphenoxy))-1-ethoxy)-4-(N'-methoxycarbonylmethyl)aminobenzaldehyde

: 404335-93-9
dihydro-fluozin-3, trimethyl ester

Guidance literature:: With methanesulfonic acid;
DOI:10.1021/ja011774y

Reference yield:

: 704-14-3
3-methoxy-6-nitro-phenol

: 404335-93-9
dihydro-fluozin-3, trimethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / potassium carbonate / dimethylformamide / 3 h / 100 °C

2: 49 percent / H₂ / platinum oxide / ethyl acetate; methanol; 1,2-dichloro-ethane / 8 h / 1034.32 Torr

3: 40 percent / diisopropylethylamine / dimethylformamide / 90 °C

4: 98 percent / methanesulfonic acid

With methanesulfonic acid; hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; platinum(IV) oxide; In methanol; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/ja011774y

Reference yield:

: 704-13-2
5-formyl-2-nitrophenol

: 404335-93-9
dihydro-fluozin-3, trimethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 77 percent / potassium carbonate / dimethylformamide / 2 h / 100 °C

2: 97 percent / p-toluenesulfonic acid / 24 h / Heating

3: 88 percent / potassium carbonate / dimethylformamide / 3 h / 100 °C

4: 49 percent / H₂ / platinum oxide / ethyl acetate; methanol; 1,2-dichloro-ethane / 8 h / 1034.32 Torr

5: 40 percent / diisopropylethylamine / dimethylformamide / 90 °C

6: 98 percent / methanesulfonic acid

With methanesulfonic acid; hydrogen; potassium carbonate; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; platinum(IV) oxide; In methanol; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/ja011774y