tert-butyl (2-methylene-3-oxo-1-(4-(trifluoromethyl)phenyl)butyl) carbonate

Base Information

Chemical Name:tert-butyl (2-methylene-3-oxo-1-(4-(trifluoromethyl)phenyl)butyl) carbonate
CAS No.:1308286-05-6
Molecular Formula:C₁₇H₁₉F₃O₄
Molecular Weight:344.331
Hs Code.:

Synonyms:tert-butyl (2-methylene-3-oxo-1-(4-(trifluoromethyl)phenyl)butyl) carbonate

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Chemical Property of tert-butyl (2-methylene-3-oxo-1-(4-(trifluoromethyl)phenyl)butyl) carbonate

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Technology Process of tert-butyl (2-methylene-3-oxo-1-(4-(trifluoromethyl)phenyl)butyl) carbonate

There total 1 articles about tert-butyl (2-methylene-3-oxo-1-(4-(trifluoromethyl)phenyl)butyl) carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 3-(α-hydroxy-p-trifluoromethylbenzyl)but-3-en-2-one

: 1308286-05-6
tert-butyl (2-methylene-3-oxo-1-(4-(trifluoromethyl)phenyl)butyl) carbonate

Guidance literature:: With dmap; In dichloromethane; at 20 ℃;
DOI:10.1039/c1ob00017a

Reference yield: 87.0%

: 4712-55-4
diphenyl hydrogen phosphite

: 1308286-05-6
tert-butyl (2-methylene-3-oxo-1-(4-(trifluoromethyl)phenyl)butyl) carbonate

: diphenyl (2-methylene-3-oxo-1-(4-(trifluoromethyl)phenyl)butyl)phosphonate

Guidance literature:: With 1-(2'-(diphenylphosphino)-[1,1'-binaphthalen]-2-yl)-3-((R)-(2-hydroxynaphthalen-1-yl)(phenyl)methyl)thiourea; In dichloromethane; at 0 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1002/ejoc.201101365

Reference yield: 86.0%

: 1308286-05-6
tert-butyl (2-methylene-3-oxo-1-(4-(trifluoromethyl)phenyl)butyl) carbonate

: 1394250-04-4
methyl 4,4-dicyano-2-methylene-3-p-tolylbut-3-enoate

: 1394249-95-6
C₂₇H₂₁F₃N₂O₃

Guidance literature:: With C₆₂H₄₃N₂PS; In toluene; at 20 ℃; for 48h; optical yield given as %ee; enantioselective reaction; Molecular sieve;
DOI:10.1039/c2cc34619b