C₁₆H₂₄O₂

Base Information

Chemical Name:C₁₆H₂₄O₂
CAS No.:1589590-44-2
Molecular Formula:C₁₆H₂₄O₂
Molecular Weight:248.365
Hs Code.:

C<sub>16</sub>H<sub>24</sub>O<sub>2</sub>

Synonyms:C₁₆H₂₄O₂

Suppliers and Price of C₁₆H₂₄O₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₆H₂₄O₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₆H₂₄O₂

There total 1 articles about C₁₆H₂₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 626-20-0
3-methoxystyrene

: 93782-92-4
(E)-6-iodo-5-methylhex-5-en-1-ol

: 1589590-44-2
C₁₆H₂₄O₂

Guidance literature:: 3-methoxystyrene; With 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; at -20 - 20 ℃; Inert atmosphere;

(E)-6-iodo-5-methylhex-5-en-1-ol; With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium hydroxide; In tetrahydrofuran; water; at -20 ℃; Inert atmosphere;
DOI:10.1021/ol500623w

Reference yield: 94.0%

: 1589590-44-2
C₁₆H₂₄O₂

: 1424371-49-2
C₁₆H₂₂O₂

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In 1,2-dichloro-ethane; at 80 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol500623w

Reference yield:

: 1589590-44-2
C₁₆H₂₄O₂

: 469-83-0,109428-81-1
(+/-)-cafestol

Guidance literature:: Multi-step reaction with 19 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / 1,2-dichloro-ethane / 3 h / 80 °C / Inert atmosphere

2.1: diethylaluminium chloride / dichloromethane / 14 h / -78 °C / Inert atmosphere

3.1: tert-butyl alcohol; lithium; ammonia / tetrahydrofuran / 6 h / -78 °C

4.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0.5 h / 0 °C / Inert atmosphere

5.1: 5,5-dimethyl-1,3-cyclohexadiene / 13 h / 160 °C / Sealed tube; Inert atmosphere

6.1: iodine / tetrahydrofuran; water / 0 - 20 °C

7.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 5 h / Reflux; Inert atmosphere

8.1: 2,6-dimethylpyridine / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

9.1: diisobutylaluminium hydride / dichloromethane / 0.67 h / -78 °C / Inert atmosphere

10.1: samarium diiodide; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran; methanol / -78 - -40 °C / Inert atmosphere

11.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

12.1: potassium tert-butylate / tetrahydrofuran; toluene / 1 h / 20 °C / Inert atmosphere

12.2: 4 h / 100 °C / Inert atmosphere

13.1: sodium hydride; 1H-imidazole / tetrahydrofuran / 3 h / Reflux; Inert atmosphere

13.2: 1 h / Reflux; Inert atmosphere

14.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 72 h / Reflux

15.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0.33 h / 0 °C

16.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.33 h / -78 °C / Inert atmosphere

16.2: MoO₅(py)(HMPA) / 1.5 h / -25 °C / Inert atmosphere

17.1: tetrahydrofuran / 0.33 h / 0 °C

18.1: (triphenylphosphine)gold(I) chloride; silver tetrafluoroborate / dichloromethane / 20 °C

19.1: osmium(VIII) oxide / tetrahydrofuran; pyridine / 0 - 20 °C

With 1H-imidazole; 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; osmium(VIII) oxide; silver tetrafluoroborate; samarium diiodide; (triphenylphosphine)gold(I) chloride; cerium(III) chloride heptahydrate; potassium tert-butylate; tetrabutyl ammonium fluoride; ammonia; iodine; diethylaluminium chloride; lithium; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium hexamethyldisilazane; tert-butyl alcohol; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; pyridine; methanol; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; 3.1: |Birch Reduction / 4.1: |Luche Cerium Reduction / 5.1: |Eschenmoser-Claisen Rearrangement / 12.1: |Wittig Olefination / 13.2: |Barton-McCombie Deoxygenation;
DOI:10.1021/ol500623w